p-methoxyphenyl 2,3-anhydro-6-O-(tert-butyldimethylsilyl)-α-D-allopyranoside

Base Information

Chemical Name:p-methoxyphenyl 2,3-anhydro-6-O-(tert-butyldimethylsilyl)-α-D-allopyranoside
CAS No.:1449491-86-4
Molecular Formula:C₁₉H₃₀O₆Si
Molecular Weight:382.529
Hs Code.:

Synonyms:p-methoxyphenyl 2,3-anhydro-6-O-(tert-butyldimethylsilyl)-α-D-allopyranoside

Suppliers and Price of p-methoxyphenyl 2,3-anhydro-6-O-(tert-butyldimethylsilyl)-α-D-allopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of p-methoxyphenyl 2,3-anhydro-6-O-(tert-butyldimethylsilyl)-α-D-allopyranoside

Chemical Property:

Purity/Quality:: 95%-98% ^*data from raw suppliers

Safty Information:

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Technology Process of p-methoxyphenyl 2,3-anhydro-6-O-(tert-butyldimethylsilyl)-α-D-allopyranoside

There total 3 articles about p-methoxyphenyl 2,3-anhydro-6-O-(tert-butyldimethylsilyl)-α-D-allopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1449491-88-6
p-methoxyphenyl 2,3-anhydro-α-D-allopyranoside

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1449491-86-4
p-methoxyphenyl 2,3-anhydro-6-O-(tert-butyldimethylsilyl)-α-D-allopyranoside

Guidance literature:: With 1H-imidazole; In dichloromethane; at 0 ℃; for 4h;
DOI:10.1016/j.tet.2013.07.018

Reference yield: 72.0%

: 157430-16-5
C₁₉H₃₀O₅Si

: 1449491-86-4
p-methoxyphenyl 2,3-anhydro-6-O-(tert-butyldimethylsilyl)-α-D-allopyranoside

: 1449491-87-5
p-methoxyphenyl 2,3-anhydro-6-O-(tert-butyldimethylsilyl)-α-D-mannopyranoside

Guidance literature:: With urea hydrogen peroxide adduct; potassium hydrogencarbonate; In acetonitrile; at 40 ℃; for 70.5h;
DOI:10.1016/j.tet.2013.07.018

Reference yield:

: 197449-36-8
p-methoxyphenyl 2,3-dideoxy-α-D-erythro-hex-2-enopyranoside

: 1449491-86-4
p-methoxyphenyl 2,3-anhydro-6-O-(tert-butyldimethylsilyl)-α-D-allopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydrogencarbonate; dihydrogen peroxide / acetonitrile / 4 h / 20 °C

2: 1H-imidazole / dichloromethane / 4 h / 0 °C

With 1H-imidazole; dihydrogen peroxide; potassium hydrogencarbonate; In dichloromethane; acetonitrile;
DOI:10.1016/j.tet.2013.07.018