(Z)-1,2-dichloro-1-o-tolylsulfanyl-ethene

Base Information

• Chemical Name: (Z)-1,2-dichloro-1-o-tolylsulfanyl-ethene
• CAS No.: 107521-67-5
• Molecular Formula: C₉H₈Cl₂S
• Molecular Weight: 219.135
• Mol file: 107521-67-5.mol

Synonyms:(Z)-1,2-dichloro-1-o-tolylsulfanyl-ethene

Chemical Property of (Z)-1,2-dichloro-1-o-tolylsulfanyl-ethene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (Z)-1,2-dichloro-1-o-tolylsulfanyl-ethene

There total 2 articles about (Z)-1,2-dichloro-1-o-tolylsulfanyl-ethene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chloroacetylene (593-63-5) + 2-methylbenzenesulfenyl chloride (14664-64-3) → (Z)-1,2-dichloro-1-o-tolylsulfanyl-ethene (107521-67-5)

Guidance literature:

With ethyl acetate;

Reference yield:

sodium ethanolate (141-52-6) + 2-thiocresol (137-06-4) → (E)-1,2-dichloro-1-o-tolylsulfanyl-ethene (107521-67-5)

Guidance literature:

With ethanol; anschliessend Erwaermen mit Dichloracetylen in Aether;

Reference yield:

(E)-1,2-dichloro-1-o-tolylsulfanyl-ethene (107521-67-5) → (E)-1-chloro-1-(toluene-2-sulfonyl)-2-o-tolylsulfanyl-ethene (877036-81-2)

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous H₂O₂; acetic acid; H₂SO₄

2: NaHCO₃; methanol

With methanol; sulfuric acid; dihydrogen peroxide; sodium hydrogencarbonate; acetic acid;

upstream raw materials:

sodium ethanolate

2-thiocresol

chloroacetylene

2-methylbenzenesulfenyl chloride

Downstream raw materials:

(Z)-1,2-dichloro-1-(toluene-2-sulfonyl)-ethene

cis-1-(toluene-2-sulfonyl)-2-o-tolylsulfanyl-ethene

(E)-1-chloro-1-(toluene-2-sulfonyl)-2-o-tolylsulfanyl-ethene

(E)-1-chloro-1,2-bis-(toluene-2-sulfonyl)-ethene