[N,N'-bis(pentafluorophenyl)ethane-1,2-diaminato]dipyridineplatinum(II)

Base Information

Chemical Name:[N,N'-bis(pentafluorophenyl)ethane-1,2-diaminato]dipyridineplatinum(II)
CAS No.:92181-60-7
Molecular Formula:C₂₄H₁₄F₁₀N₄Pt
Molecular Weight:743.466
Hs Code.:

Synonyms:[N,N'-bis(pentafluorophenyl)ethane-1,2-diaminato]dipyridineplatinum(II)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [N,N'-bis(pentafluorophenyl)ethane-1,2-diaminato]dipyridineplatinum(II)

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Technology Process of [N,N'-bis(pentafluorophenyl)ethane-1,2-diaminato]dipyridineplatinum(II)

There total 2 articles about [N,N'-bis(pentafluorophenyl)ethane-1,2-diaminato]dipyridineplatinum(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 110-86-1
pyridine

: 14096-51-6
dichloro(ethylenediamine)platinum(II)

: 392-56-3
Hexafluorobenzene

: 92181-60-7
[N,N'-bis(pentafluorophenyl)ethane-1,2-diaminato]dipyridineplatinum(II)

: 124-38-9,18923-20-1
carbon dioxide

Guidance literature:: With Tl₂CO₃; In pyridine; N2-atmosphere; stirring (120°C, 1 h); evapn. (vac.), light petroleum addn., stirring (1 h), decanting, extg. (Me2CO), filtering, concg., light petroleum addn., crystn. on concg., re crystn. (Me2CO / light petroleum);
DOI:10.1016/S0277-5387(97)00310-0

Reference yield: 44.0%

: 14096-51-6
dichloro(ethylenediamine)platinum(II)

: 392-56-3
Hexafluorobenzene

: 92181-60-7
[N,N'-bis(pentafluorophenyl)ethane-1,2-diaminato]dipyridineplatinum(II)

Guidance literature:: With pyridine; In pyridine; byproducts: TlCl, CO2, 1,2,4,5-tetrafluorobenzene; TlO2C(p-HC6F4) and Pt(en)Cl2 and C6F6 were stirred together in pyridineat 115°C for 20 min; further byproduct: C5H5NHF;; pyridine was evapd., residue was stirred with light petroleum to removetraces of pyridine, then was extd. with acetone, extract was filtered, residue was evapd. and crystd.; elem. anal.;