N-(2-iodo-phenyl)-N-[1-(toluene-4-sulfonylmethyl)-hex-1-enyl]-formamide

Base Information

Chemical Name:N-(2-iodo-phenyl)-N-[1-(toluene-4-sulfonylmethyl)-hex-1-enyl]-formamide
CAS No.:514805-25-5
Molecular Formula:C₂₁H₂₄INO₃S
Molecular Weight:497.397
Hs Code.:

<i>N</i>-(2-iodo-phenyl)-<i>N</i>-[1-(toluene-4-sulfonylmethyl)-hex-1-enyl]-formamide

Synonyms:N-(2-iodo-phenyl)-N-[1-(toluene-4-sulfonylmethyl)-hex-1-enyl]-formamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-iodo-phenyl)-N-[1-(toluene-4-sulfonylmethyl)-hex-1-enyl]-formamide

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Technology Process of N-(2-iodo-phenyl)-N-[1-(toluene-4-sulfonylmethyl)-hex-1-enyl]-formamide

There total 1 articles about N-(2-iodo-phenyl)-N-[1-(toluene-4-sulfonylmethyl)-hex-1-enyl]-formamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 10113-39-0
N-formyl-2-iodoaniline

: 82721-81-1
1-(p-toluenesulfonyl)-1-heptyne

: 514805-25-5
N-(2-iodo-phenyl)-N-[1-(toluene-4-sulfonylmethyl)-hex-1-enyl]-formamide

Guidance literature:: With potassium carbonate; In water; N,N-dimethyl-formamide; at 20 ℃; for 192h;
DOI:10.1021/jo026595t

Reference yield: 94.0%

: 67-56-1
methanol

: 201230-82-2
carbon monoxide

: 514805-25-5
N-(2-iodo-phenyl)-N-[1-(toluene-4-sulfonylmethyl)-hex-1-enyl]-formamide

: 514805-20-0
2-{Formyl-[(E)-1-(toluene-4-sulfonylmethyl)-hex-1-enyl]-amino}-benzoic acid methyl ester

Guidance literature:: With triethylamine; palladium diacetate; at 70 ℃; for 48h; under 20520 Torr;
DOI:10.1021/jo026595t

Reference yield:

: 514805-25-5
N-(2-iodo-phenyl)-N-[1-(toluene-4-sulfonylmethyl)-hex-1-enyl]-formamide

: 4-oxo-2-pentylidene-3-(toluene-4-sulfonyl)-3,4-dihydro-2H-quinoline-1-carbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / triethylamine / Pd(OAc)2 / 48 h / 70 °C / 20520 Torr

2: 77 percent / LiHMDS / tetrahydrofuran / 1.17 h / -78 °C

With triethylamine; lithium hexamethyldisilazane; palladium diacetate; In tetrahydrofuran;
DOI:10.1021/jo026595t