methyl 4-(N-(tert-butoxycarbonyl)-2-(dimethylamino)-ethylsulfonamido)-3-(cyclopropylmethoxy)benzoate

Base Information

Chemical Name:methyl 4-(N-(tert-butoxycarbonyl)-2-(dimethylamino)-ethylsulfonamido)-3-(cyclopropylmethoxy)benzoate
CAS No.:1610861-32-9
Molecular Formula:C₂₁H₃₂N₂O₇S
Molecular Weight:456.56
Hs Code.:

Synonyms:methyl 4-(N-(tert-butoxycarbonyl)-2-(dimethylamino)-ethylsulfonamido)-3-(cyclopropylmethoxy)benzoate

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Chemical Property of methyl 4-(N-(tert-butoxycarbonyl)-2-(dimethylamino)-ethylsulfonamido)-3-(cyclopropylmethoxy)benzoate

Chemical Property:

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Technology Process of methyl 4-(N-(tert-butoxycarbonyl)-2-(dimethylamino)-ethylsulfonamido)-3-(cyclopropylmethoxy)benzoate

There total 6 articles about methyl 4-(N-(tert-butoxycarbonyl)-2-(dimethylamino)-ethylsulfonamido)-3-(cyclopropylmethoxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1610861-33-0
methyl 3-(cyclopropylmethoxy)-4-(2-(dimethylamino)-ethylsulfonamido)benzoate

: 1610861-32-9
methyl 4-(N-(tert-butoxycarbonyl)-2-(dimethylamino)-ethylsulfonamido)-3-(cyclopropylmethoxy)benzoate

Guidance literature:: With dmap; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 619-14-7
3-hydroxy-4-nitro-benzoic acid

: 1610861-32-9
methyl 4-(N-(tert-butoxycarbonyl)-2-(dimethylamino)-ethylsulfonamido)-3-(cyclopropylmethoxy)benzoate

Guidance literature:: Multi-step reaction with 6 steps

1: sulfuric acid / water / 144 h / 60 °C

2: potassium iodide; potassium carbonate / N,N-dimethyl-formamide / 50 °C / Inert atmosphere

3: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 775.74 Torr

4: pyridine / dichloromethane / 1 h / 0 - 20 °C

5: ethanol / 1 h / 20 °C

6: dmap / dichloromethane / 1 h / 20 °C

With pyridine; dmap; sulfuric acid; palladium 10% on activated carbon; hydrogen; potassium carbonate; potassium iodide; In methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 713-52-0
methyl 3-hydroxy-4-nitrobenzoate

: 1610861-32-9
methyl 4-(N-(tert-butoxycarbonyl)-2-(dimethylamino)-ethylsulfonamido)-3-(cyclopropylmethoxy)benzoate

Guidance literature:: Multi-step reaction with 5 steps

1: potassium iodide; potassium carbonate / N,N-dimethyl-formamide / 50 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 775.74 Torr

3: pyridine / dichloromethane / 1 h / 0 - 20 °C

4: ethanol / 1 h / 20 °C

5: dmap / dichloromethane / 1 h / 20 °C

With pyridine; dmap; palladium 10% on activated carbon; hydrogen; potassium carbonate; potassium iodide; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;