2-[bis(3,4-dimethoxyphenyl)methyl]-5,6-dimethoxy-1H-indene-1,3(2H)-dione

Base Information

Chemical Name:2-[bis(3,4-dimethoxyphenyl)methyl]-5,6-dimethoxy-1H-indene-1,3(2H)-dione
CAS No.:738616-29-0
Molecular Formula:C₂₈H₂₈O₈
Molecular Weight:492.526
Hs Code.:

Synonyms:2-[bis(3,4-dimethoxyphenyl)methyl]-5,6-dimethoxy-1H-indene-1,3(2H)-dione

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Chemical Property of 2-[bis(3,4-dimethoxyphenyl)methyl]-5,6-dimethoxy-1H-indene-1,3(2H)-dione

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Technology Process of 2-[bis(3,4-dimethoxyphenyl)methyl]-5,6-dimethoxy-1H-indene-1,3(2H)-dione

There total 5 articles about 2-[bis(3,4-dimethoxyphenyl)methyl]-5,6-dimethoxy-1H-indene-1,3(2H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 36517-91-6
2,3-dihydro-5,6-dimethoxy-1H-indene-1,3-dione

: 74084-26-7
3,3',4,4'-tetramethoxybenzhydrole

: 738616-29-0
2-[bis(3,4-dimethoxyphenyl)methyl]-5,6-dimethoxy-1H-indene-1,3(2H)-dione

Guidance literature:: With toluene-4-sulfonic acid; In dichloromethane; toluene; for 18h; Reflux;
DOI:10.1039/c8cc10122a

Reference yield:

: 91-16-7
1,2-dimethoxybenzene

: 738616-29-0
2-[bis(3,4-dimethoxyphenyl)methyl]-5,6-dimethoxy-1H-indene-1,3(2H)-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / polyphosphoric acid / 0.5 h / 80 °C

2: 92 percent / pyridine; hydrogen / Pd/C / methanol / 168 h / 20 °C / 4500.45 Torr

3: 81 percent / para-toluenesulfonic acid monohydrate / benzene; 1,2-dichloro-ethane / 2 h / Heating

With pyridine; PPA; hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In methanol; 1,2-dichloro-ethane; benzene;
DOI:10.1002/ejoc.200300782

Reference yield:

: 4131-03-7
bis(3,4-dimethoxyphenyl)methanone

: 738616-29-0
2-[bis(3,4-dimethoxyphenyl)methyl]-5,6-dimethoxy-1H-indene-1,3(2H)-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / pyridine; hydrogen / Pd/C / methanol / 168 h / 20 °C / 4500.45 Torr

2: 81 percent / para-toluenesulfonic acid monohydrate / benzene; 1,2-dichloro-ethane / 2 h / Heating

With pyridine; hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In methanol; 1,2-dichloro-ethane; benzene;
DOI:10.1002/ejoc.200300782