Methyl alpha-D-galactopyranosiduronic acid

Base Information

• Chemical Name: Methyl alpha-D-galactopyranosiduronic acid
• CAS No.: 5155-53-3
• Molecular Formula: C₇H₁₂O₇
• Molecular Weight: 208.168
• DSSTox Substance ID: DTXSID401031448
• Nikkaji Number: J1.025.882K

Synonyms:Methyl alpha-D-galactopyranosiduronic acid;DTXSID401031448;5155-53-3

Chemical Property of Methyl alpha-D-galactopyranosiduronic acid

Chemical Property:

• XLogP3: -1.8
• Hydrogen Bond Donor Count: 4
• Hydrogen Bond Acceptor Count: 7
• Rotatable Bond Count: 2
• Exact Mass: 208.05830272
• Heavy Atom Count: 14
• Complexity: 218

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: COC1C(C(C(C(O1)C(=O)O)O)O)O
• Isomeric SMILES: CO[C@@H]1[C@@H]([C@H]([C@H]([C@H](O1)C(=O)O)O)O)O

Technology Process of Methyl alpha-D-galactopyranosiduronic acid

There total 24 articles about Methyl alpha-D-galactopyranosiduronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl beta-D-glucopyranoside (709-50-2) → formic acid (64-18-6) + glycolic Acid (79-14-1) + LACTIC ACID (849585-22-4,106989-11-1,26811-96-1,31587-11-8,26100-51-6) + glyceric acid (473-81-4,118916-26-0) + oxalic acid (144-62-7,97993-78-7) + acetic acid (64-19-7,77671-22-8) + methyl β-D-glucopyranosiduronic acid (4356-84-7,5155-45-3,5155-53-3,5241-02-1,5391-16-2,18486-39-0,46325-26-2,46325-27-3,73410-95-4,99094-38-9,134355-30-9,135414-77-6)

Guidance literature:

With oxygen; sodium hydroxide; In water; at 50 ℃; pH=13;

DOI:10.1016/j.catcom.2019.105895

Reference yield:

licorice-saponin A3 (118325-22-7) → glycyrrhetic acid + methyl beta-D-glucopyranoside (709-50-2) + methyl β-D-glucopyranosiduronic acid (4356-84-7,5155-45-3,5155-53-3,5241-02-1,5391-16-2,18486-39-0,46325-26-2,46325-27-3,73410-95-4,99094-38-9,134355-30-9,135414-77-6)

Guidance literature:

With hydrogenchloride; In methanol;

DOI:10.1248/cpb.36.3710

Reference yield:

licorice-saponin D3 (118536-87-1) → (2R,4R,4aR,6aS,6bR,8aR,10S,12aR,14bS)-4-Acetoxy-10-hydroxy-2,4a,6a,6b,9,9,12a-heptamethyl-1,2,3,4,4a,5,6,6a,6b,7,8,8a,9,10,11,12,12a,12b,13,14b-icosahydro-picene-2-carboxylic acid (118525-50-1) + methyl 6-deoxy-α-L-mannopyranoside (14917-55-6) + methyl β-D-glucopyranosiduronic acid (4356-84-7,5155-45-3,5155-53-3,5241-02-1,5391-16-2,18486-39-0,46325-26-2,46325-27-3,73410-95-4,99094-38-9,134355-30-9,135414-77-6)

Guidance literature:

methanolysis;

DOI:10.1248/cpb.36.3710

upstream raw materials:

C₄₄H₆₄O₁₆

licorice-saponin D₃

licorice-saponin A₃

methyl beta-D-glucopyranoside

Downstream raw materials:

benzyl (methyl 2,3,4-tri-O-benzyl-α-D-galactopyranoside)uronate

methyl (methyl α-D-galacturonopyranoside)uronate

L-galactonic acid

methyl 2-acetamido-4-azido-3-O-(benzyl 2,3,4-tri-O-benzyl-α-D-galactopyranosyluronate)-2,4,6-trideoxy-α-D-galactopyranoside

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