Technology Process of C23H29N5O3
There total 8 articles about C23H29N5O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C31H45N5O7;
With
sodium dithionite;
In
tetrahydrofuran; ethanol; water;
at 60 ℃;
oxalyl dichloride;
With
triethylamine;
In
dichloromethane;
for 2h;
With
trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
for 16h;
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
for 16h;
DOI:10.1021/jm400815m
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: butan-1-ol; N,N-dimethyl-formamide / 0.75 h / 130 °C / Microwave irradiation
2.1: nitric acid; sulfuric acid / -10 °C
3.1: dmap; triethylamine / tetrahydrofuran / 2.5 h / 20 °C
4.1: triethylamine / tetrahydrofuran / 1 h / 50 °C
5.1: sodium dithionite / ethanol; water; tetrahydrofuran / 60 °C
5.2: 2 h
5.3: 16 h / 20 °C
With
dmap; sodium dithionite; sulfuric acid; nitric acid; triethylamine;
In
tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; butan-1-ol;