C₁₉H₂₇Cl₂NO₃Si

Base Information Edit

Chemical Name:C₁₉H₂₇Cl₂NO₃Si
CAS No.:1268246-35-0
Molecular Formula:C₁₉H₂₇Cl₂NO₃Si
Molecular Weight:416.42
Hs Code.:
Mol file:1268246-35-0.mol

C<sub>19</sub>H<sub>27</sub>Cl<sub>2</sub>NO<sub>3</sub>Si

Synonyms:C₁₉H₂₇Cl₂NO₃Si

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Chemical Property of C₁₉H₂₇Cl₂NO₃Si Edit

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Technology Process of C₁₉H₂₇Cl₂NO₃Si

There total 10 articles about C₁₉H₂₇Cl₂NO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.2%

: 1268246-34-9
C₁₈H₂₃Cl₂NO₃Si

: 676-58-4
methylmagnesium chloride

: 1268246-35-0
C₁₉H₂₇Cl₂NO₃Si

Guidance literature:: C₁₈H₂₃Cl₂NO₃Si; methylmagnesium chloride; In tetrahydrofuran; at -30 - -20 ℃; for 3.5h; Inert atmosphere;

With water; ammonium chloride; In tetrahydrofuran;

Reference yield:

: 278597-30-1
[3-(2,6-dichlorophenyl)-5-(propan-2-yl)-1,2-oxazol-4-yl]methanol

: 1268246-35-0
C₁₉H₂₇Cl₂NO₃Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / dichloromethane / 20 °C

2.1: N-Bromosuccinimide / tetrachloromethane / 1 h / Reflux

3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 20 °C

3.2: 0.5 h / 20 °C

4.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 - 20 °C

5.1: osmium(VIII) oxide; 2,6-dimethylpyridine; sodium periodate / 1,4-dioxane; water / 2 h / 20 °C

6.1: tetrahydrofuran / 3.5 h / -30 - -20 °C / Inert atmosphere

With 2,6-dimethylpyridine; sodium periodate; N-Bromosuccinimide; osmium(VIII) oxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 1,4-dioxane; tetrachloromethane; dichloromethane; water;

Reference yield:

: 83-38-5
2,6-dichlorobenzaldehyde

: 1268246-35-0
C₁₉H₂₇Cl₂NO₃Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: hydroxylamine hydrochloride; sodium hydroxide / ethanol; water / 24 h / 90 °C

2.1: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 20 °C

3.1: sodium methylate / tetrahydrofuran; methanol / 16 h / 20 °C

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

4.2: 0.17 h / 0 °C

5.1: triethylamine / dichloromethane / 20 °C

6.1: N-Bromosuccinimide / tetrachloromethane / 1 h / Reflux

7.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 20 °C

7.2: 0.5 h / 20 °C

8.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 - 20 °C

9.1: osmium(VIII) oxide; 2,6-dimethylpyridine; sodium periodate / 1,4-dioxane; water / 2 h / 20 °C

10.1: tetrahydrofuran / 3.5 h / -30 - -20 °C / Inert atmosphere

With 2,6-dimethylpyridine; sodium periodate; N-chloro-succinimide; N-Bromosuccinimide; osmium(VIII) oxide; lithium aluminium tetrahydride; hydroxylamine hydrochloride; sodium methylate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; tetrachloromethane; ethanol; dichloromethane; water; N,N-dimethyl-formamide;