cis-2-<(p-methoxyphenyl)oxy>-5-(chloromethyl)-5-methyl-2-oxo-1,3,2-dioxaphosphorinane

Base Information

Chemical Name:cis-2-<(p-methoxyphenyl)oxy>-5-(chloromethyl)-5-methyl-2-oxo-1,3,2-dioxaphosphorinane
CAS No.:36912-31-9
Molecular Formula:C₁₂H₁₆ClO₅P
Molecular Weight:306.683
Hs Code.:

Synonyms:cis-2-<(p-methoxyphenyl)oxy>-5-(chloromethyl)-5-methyl-2-oxo-1,3,2-dioxaphosphorinane

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Chemical Property of cis-2-<(p-methoxyphenyl)oxy>-5-(chloromethyl)-5-methyl-2-oxo-1,3,2-dioxaphosphorinane

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Technology Process of cis-2-<(p-methoxyphenyl)oxy>-5-(chloromethyl)-5-methyl-2-oxo-1,3,2-dioxaphosphorinane

There total 9 articles about cis-2-<(p-methoxyphenyl)oxy>-5-(chloromethyl)-5-methyl-2-oxo-1,3,2-dioxaphosphorinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28097-07-6
trans-2-chloro-5-methyl-1,3,2-dioxaphosphorinane-r-5-methyl chloride 2-oxide

: 36912-31-9
cis-2-<(p-methoxyphenyl)oxy>-5-(chloromethyl)-5-methyl-2-oxo-1,3,2-dioxaphosphorinane

Guidance literature:: Multi-step reaction with 3 steps

1: CsF / tetrahydrofuran

2: tetrabutylammonium fluoride / tetrahydrofuran

3: CsF / tetrahydrofuran

With tetrabutyl ammonium fluoride; cesium fluoride; In tetrahydrofuran;
DOI:10.1021/ja00316a041

Reference yield:

: 36912-34-2
trans-2-(p-methylphenoxy)-5-(chloromethyl)-5-methyl-2-oxo-1,3,2-dioxaphosphorinane

: 36912-31-9
cis-2-<(p-methoxyphenyl)oxy>-5-(chloromethyl)-5-methyl-2-oxo-1,3,2-dioxaphosphorinane

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutylammonium fluoride / tetrahydrofuran

2: CsF / tetrahydrofuran

With tetrabutyl ammonium fluoride; cesium fluoride; In tetrahydrofuran;
DOI:10.1021/ja00316a041

Reference yield:

: 343863-92-3
5-Chloromethyl-2-fluoro-5-methyl-[1,3,2]dioxaphosphinane 2-oxide

: 36912-31-9
cis-2-<(p-methoxyphenyl)oxy>-5-(chloromethyl)-5-methyl-2-oxo-1,3,2-dioxaphosphorinane

Guidance literature:: Multi-step reaction with 3 steps

1: CsF / tetrahydrofuran

2: tetrabutylammonium fluoride / tetrahydrofuran

3: CsF / tetrahydrofuran

With tetrabutyl ammonium fluoride; cesium fluoride; In tetrahydrofuran;
DOI:10.1021/ja00316a041