para-methylphenyl 4,6-O-benzylidene-3-O-para-methoxybenzyl-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:para-methylphenyl 4,6-O-benzylidene-3-O-para-methoxybenzyl-1-thio-β-D-glucopyranoside
CAS No.:942043-53-0
Molecular Formula:C₂₈H₃₀O₆S
Molecular Weight:494.609
Hs Code.:

Synonyms:para-methylphenyl 4,6-O-benzylidene-3-O-para-methoxybenzyl-1-thio-β-D-glucopyranoside

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Chemical Property of para-methylphenyl 4,6-O-benzylidene-3-O-para-methoxybenzyl-1-thio-β-D-glucopyranoside

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Technology Process of para-methylphenyl 4,6-O-benzylidene-3-O-para-methoxybenzyl-1-thio-β-D-glucopyranoside

There total 12 articles about para-methylphenyl 4,6-O-benzylidene-3-O-para-methoxybenzyl-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 123-11-5
4-methoxy-benzaldehyde

: 219518-19-1
4-methylphenyl 4,6-O-benzylidene-1-thio-β-D-glucopyranoside

: 942043-53-0
para-methylphenyl 4,6-O-benzylidene-3-O-para-methoxybenzyl-1-thio-β-D-glucopyranoside

Guidance literature:: 4-methylphenyl 4,6-O-benzylidene-1-thio-β-D-glucopyranoside; With chloro-trimethyl-silane; triethylamine; In dichloromethane; at 20 ℃; for 9h; Cooling with ice;

4-methoxy-benzaldehyde; With triethylsilane; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -30 - 20 ℃; for 8h; Molecular sieve;

With tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane;

Reference yield: 88.0%

: 824-94-2
p-methoxybenzyl chloride

: 219518-19-1
4-methylphenyl 4,6-O-benzylidene-1-thio-β-D-glucopyranoside

: 942043-53-0
para-methylphenyl 4,6-O-benzylidene-3-O-para-methoxybenzyl-1-thio-β-D-glucopyranoside

Guidance literature:: 4-methylphenyl 4,6-O-benzylidene-1-thio-β-D-glucopyranoside; With di(n-butyl)tin oxide; In toluene; Inert atmosphere; Reflux; Dean-Stark;

p-methoxybenzyl chloride; With tetrabutylammomium bromide; cesium fluoride; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1021/acs.joc.0c01404

Reference yield: 82.0%

: 942043-17-6
4-methylphenyl 2,3,4,6-tetrakis-O-trimethylsilyl-1-thio-β-D-glucopyranoside

: 53448-06-9,58838-14-5,5604-55-7
pent-3-enal

: 100-52-7
benzaldehyde

: 123-11-5
4-methoxy-benzaldehyde

: 66-99-9
β-naphthaldehyde

: 942043-54-1
p-methylphenyl 4,6-O-benzylidine-3-O-(naphthalen-2-ylmethyl)-1-thio-β-D-glucopyranoside

: 1012064-99-1
C₂₅H₃₀O₅S

: 942043-53-0
para-methylphenyl 4,6-O-benzylidene-3-O-para-methoxybenzyl-1-thio-β-D-glucopyranoside

: 4-methylphenyl 3-O-benzyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

Guidance literature:: 4-methylphenyl 2,3,4,6-tetrakis-O-trimethylsilyl-1-thio-β-D-glucopyranoside; benzaldehyde; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -86 ℃; for 2h; Molecular sieve;

pent-3-enal; benzaldehyde; 4-methoxy-benzaldehyde; β-naphthaldehyde; With triethylsilane; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -86 ℃; for 5h; Combinatorial reaction / High throughput screening (HTS);

With tetrabutyl ammonium fluoride; In dichloromethane; at -86 - 20 ℃;