(E)-ethyl-6-((4-(ethoxycarbonyl)phenyl)diazenyl)-[1,1’-biphenyl]-3-carboxylate

Base Information

Chemical Name:(E)-ethyl-6-((4-(ethoxycarbonyl)phenyl)diazenyl)-[1,1’-biphenyl]-3-carboxylate
CAS No.:1619236-84-8
Molecular Formula:C₂₄H₂₂N₂O₄
Molecular Weight:402.45
Hs Code.:

Synonyms:(E)-ethyl-6-((4-(ethoxycarbonyl)phenyl)diazenyl)-[1,1’-biphenyl]-3-carboxylate

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Chemical Property of (E)-ethyl-6-((4-(ethoxycarbonyl)phenyl)diazenyl)-[1,1’-biphenyl]-3-carboxylate

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Technology Process of (E)-ethyl-6-((4-(ethoxycarbonyl)phenyl)diazenyl)-[1,1’-biphenyl]-3-carboxylate

There total 3 articles about (E)-ethyl-6-((4-(ethoxycarbonyl)phenyl)diazenyl)-[1,1’-biphenyl]-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 7250-68-2,122045-06-1
(E)-diethyl 4,4′-(diazene-1,2-diyl)dibenzoate

: 100-63-0
phenylhydrazine

: 1619236-84-8
(E)-ethyl-6-((4-(ethoxycarbonyl)phenyl)diazenyl)-[1,1’-biphenyl]-3-carboxylate

Guidance literature:: With oxygen; palladium diacetate; In acetonitrile; at 60 ℃; for 24h; Sealed tube;
DOI:10.1002/cctc.201500575

Reference yield: 29.0%

: 7250-68-2,122045-06-1
(E)-diethyl 4,4′-(diazene-1,2-diyl)dibenzoate

: 94-36-0
dibenzoyl peroxide

: 1619236-84-8
(E)-ethyl-6-((4-(ethoxycarbonyl)phenyl)diazenyl)-[1,1’-biphenyl]-3-carboxylate

Guidance literature:: With palladium diacetate; In chlorobenzene; acetonitrile; at 130 ℃; for 24h; regioselective reaction; Sealed tube;
DOI:10.1039/c4ob00993b

Reference yield:

: 94-09-7
p-aminoethylbenzoate

: 1619236-84-8
(E)-ethyl-6-((4-(ethoxycarbonyl)phenyl)diazenyl)-[1,1’-biphenyl]-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; copper(I) bromide / toluene / 24 h / 60 °C

2: palladium diacetate / acetonitrile; chlorobenzene / 24 h / 130 °C / Sealed tube

With pyridine; palladium diacetate; copper(I) bromide; In chlorobenzene; toluene; acetonitrile;
DOI:10.1039/c4ob00993b