ethyl 2,2-bis(4-methoxyphenyl)acetate

Base Information

Chemical Name:ethyl 2,2-bis(4-methoxyphenyl)acetate
CAS No.:121090-64-0
Molecular Formula:C₁₈H₂₀O₄
Molecular Weight:300.354
Hs Code.:

Synonyms:ethyl 2,2-bis(4-methoxyphenyl)acetate

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Chemical Property of ethyl 2,2-bis(4-methoxyphenyl)acetate

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Technology Process of ethyl 2,2-bis(4-methoxyphenyl)acetate

There total 9 articles about ethyl 2,2-bis(4-methoxyphenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 104-92-7
1-bromo-4-methoxy-benzene

: 141-78-6
ethyl acetate

: 121090-64-0
ethyl 2,2-bis(4-methoxyphenyl)acetate

Guidance literature:: With potassium phosphate; (1,10-phenanthroline)(triphenylphosphine)CuBr; tri-tert-butylphosphonium tetrafluoroborate; palladium diacetate; In N,N-dimethyl-formamide; at 110 ℃; for 24h; Inert atmosphere;
DOI:10.1002/adsc.201100172

Reference yield: 90.0%

: 64-17-5
ethanol

: 1226-42-2
1,2-bis(4-methoxyphenyl)-1,2-ethanedione

: 121090-64-0
ethyl 2,2-bis(4-methoxyphenyl)acetate

Guidance literature:: With 5,6-bis(5-methoxythiophen-2-yl)pyrazine-2,3-dicarbonitrile; triethyl phosphite; In 1,2-dichloro-ethane; at 20 ℃; for 48h; Schlenk technique; Inert atmosphere; Irradiation; Green chemistry;
DOI:10.1002/anie.202107080

Reference yield: 73.0%

: 623-73-4
diazoacetic acid ethyl ester

: 696-62-8
para-iodoanisole

: 121090-64-0
ethyl 2,2-bis(4-methoxyphenyl)acetate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; silver carbonate; In toluene; at 20 - 65 ℃; for 16h; Schlenk technique; Inert atmosphere;
DOI:10.1021/ja513275c