C₃₁H₃₉ClF₂N₄O₂Si

Base Information Edit

Chemical Name:C₃₁H₃₉ClF₂N₄O₂Si
CAS No.:1413876-13-7
Molecular Formula:C₃₁H₃₉ClF₂N₄O₂Si
Molecular Weight:601.212
Hs Code.:
Mol file:1413876-13-7.mol

C<sub>31</sub>H<sub>39</sub>ClF<sub>2</sub>N<sub>4</sub>O<sub>2</sub>Si

Synonyms:C₃₁H₃₉ClF₂N₄O₂Si

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Chemical Property of C₃₁H₃₉ClF₂N₄O₂Si Edit

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Technology Process of C₃₁H₃₉ClF₂N₄O₂Si

There total 14 articles about C₃₁H₃₉ClF₂N₄O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1413875-84-9
5-[1-(trans-4-{[tert-butyl(dimethyl)silyl]oxy}cyclohexyl)-1H-pyrazol-4-yl]-3-[1-(2-chloro-3-fluoro-6-methoxyphenyl)-2-fluoro-2,2-bis(phenylsulfonyl)ethyl]-1H-pyrrolo[2,3-b]pyridine

: 1413876-13-7
C₃₁H₃₉ClF₂N₄O₂Si

Guidance literature:: With methanol; disodium hydrogenphosphate; sodium amalgam; at -20 - -5 ℃; for 1.5h;

Reference yield:

: 1175275-29-2
4-iodo-1-(1,4-dioxaspiro[4.5]decan-8-yl)-1H-pyrazole

: 1413876-13-7
C₃₁H₃₉ClF₂N₄O₂Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: water / pyridinium p-toluenesulfonate / acetone / 16 h / 65 °C

2.1: ethanol; sodium tetrahydroborate / 2 h / 20 °C / Inert atmosphere

3.1: 1H-imidazole / dmap / dichloromethane / 0.33 h / 20 °C

4.1: isopropylmagnesium chloride / tetrahydrofuran / 1.08 h / 0 °C / Inert atmosphere

4.2: 1 h / 20 °C

5.1: potassium fluoride / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane; water / 1.5 h / 90 °C / Inert atmosphere

6.1: disodium hydrogenphosphate; sodium amalgam; methanol / 1.5 h / -20 - -5 °C

With 1H-imidazole; methanol; potassium fluoride; sodium tetrahydroborate; disodium hydrogenphosphate; sodium amalgam; ethanol; water; isopropylmagnesium chloride; dmap; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; pyridinium p-toluenesulfonate; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; acetone;

Reference yield:

: 261762-39-4
2-chloro-3,6-difluorobenzaldehyde

: 1413876-13-7
C₃₁H₃₉ClF₂N₄O₂Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium methylate / tetrahydrofuran; methanol / 60 °C

2.1: potassium hydroxide / methanol / 12 h / 20 °C

3.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C

3.2: 1.5 h / -78 - 20 °C

4.1: potassium fluoride / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane; water / 1.5 h / 90 °C / Inert atmosphere

5.1: disodium hydrogenphosphate; sodium amalgam; methanol / 1.5 h / -20 - -5 °C

With methanol; potassium fluoride; disodium hydrogenphosphate; sodium amalgam; n-butyllithium; sodium methylate; potassium hydroxide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; 1,4-dioxane; methanol; hexane; water;