2-[4-(2-acetylamino-2-allyloxycarbonylethyl)-2-ethylphenylamino]-benzoic acid

Base Information

Chemical Name:2-[4-(2-acetylamino-2-allyloxycarbonylethyl)-2-ethylphenylamino]-benzoic acid
CAS No.:592531-95-8
Molecular Formula:C₂₃H₂₆N₂O₅
Molecular Weight:410.47
Hs Code.:

Synonyms:2-[4-(2-acetylamino-2-allyloxycarbonylethyl)-2-ethylphenylamino]-benzoic acid

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Chemical Property of 2-[4-(2-acetylamino-2-allyloxycarbonylethyl)-2-ethylphenylamino]-benzoic acid

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Technology Process of 2-[4-(2-acetylamino-2-allyloxycarbonylethyl)-2-ethylphenylamino]-benzoic acid

There total 4 articles about 2-[4-(2-acetylamino-2-allyloxycarbonylethyl)-2-ethylphenylamino]-benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: C₁₉H₁₅IO₂

: 402924-98-5
2-acetylamino-3-(4-amino-3-ethyl-phenyl)-propionic acid allyl ester

: 592531-95-8
2-[4-(2-acetylamino-2-allyloxycarbonylethyl)-2-ethylphenylamino]-benzoic acid

Guidance literature:: With copper diacetate; In isopropyl alcohol; at 80 ℃;
DOI:10.1016/S0960-894X(03)00302-0

Reference yield:

: 1488-42-2,109545-72-4
Diphenyliodonium-2-carboxylate

: 402924-98-5
2-acetylamino-3-(4-amino-3-ethyl-phenyl)-propionic acid allyl ester

: 592531-95-8
2-[4-(2-acetylamino-2-allyloxycarbonylethyl)-2-ethylphenylamino]-benzoic acid

Guidance literature:: With copper diacetate; In N,N-dimethyl-formamide; at 90 ℃; for 6h;
DOI:10.1021/jm034088d

Reference yield:

: 436864-41-4
benzyl (2E)-2-(acetylamino)-3-(4-amino-3-ethylphenyl)-2-propenoate

: 592531-95-8
2-[4-(2-acetylamino-2-allyloxycarbonylethyl)-2-ethylphenylamino]-benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / Pd/C; H₂ / methanol / 20 °C / 3040 Torr

2: 62 percent / Cs₂CO₃ / dimethylformamide / 3 h / 20 °C

3: copper(II) acetate / dimethylformamide / 6 h / 90 °C

With palladium on activated charcoal; hydrogen; copper diacetate; caesium carbonate; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm034088d