1,2-Diphenyl-1-ethoxyethylen

Base Information

Chemical Name:1,2-Diphenyl-1-ethoxyethylen
CAS No.:13676-20-5
Molecular Formula:C₁₆H₁₆O
Molecular Weight:224.302
Hs Code.:

Synonyms:1,2-Diphenyl-1-ethoxyethylen

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Chemical Property of 1,2-Diphenyl-1-ethoxyethylen

Chemical Property:

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Technology Process of 1,2-Diphenyl-1-ethoxyethylen

There total 6 articles about 1,2-Diphenyl-1-ethoxyethylen which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 591-50-4
iodobenzene

: 32569-84-9
ethoxyethynylbenzene

: 13676-20-5
1,2-Diphenyl-1-ethoxyethylen

Guidance literature:: With palladium diacetate; caesium carbonate; isopropyl alcohol; tricyclohexylphosphine tetrafluoroborate; In 1,4-dioxane; at 50 ℃; for 10h; regioselective reaction; Inert atmosphere;
DOI:10.1021/jo5002356

Reference yield:

: 451-40-1
phenyl benzyl ketone

: 74-96-4
ethyl bromide

: 16282-16-9
1,2-diphenyl-butan-1-one

: 13676-20-5
1,2-Diphenyl-1-ethoxyethylen

Guidance literature:: With sodium hydroxide; tetrabutylammomium bromide; In benzene; at 24 ℃; Rate constant; other catalysts (phase transfer catalysts) ; other solvents;
DOI:10.1021/jo00296a030

Reference yield:

: 774-48-1
(diethoxymethyl)benzene

: 13676-20-5
1,2-Diphenyl-1-ethoxyethylen

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂, AcCl

3: NaH / 1,2-dimethoxy-ethane / Heating

With thionyl chloride; sodium hydride; acetyl chloride; In 1,2-dimethoxyethane;
DOI:10.1002/jlac.19666990106