C₁₉H₃₁N₃O₆P₂

Base Information

• Chemical Name: C₁₉H₃₁N₃O₆P₂
• CAS No.: 1346258-39-6
• Molecular Formula: C₁₉H₃₁N₃O₆P₂
• Molecular Weight: 459.419
• Mol file: 1346258-39-6.mol

Synonyms:C₁₉H₃₁N₃O₆P₂

Chemical Property of C₁₉H₃₁N₃O₆P₂

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₉H₃₁N₃O₆P₂

There total 3 articles about C₁₉H₃₁N₃O₆P₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

P,P'-methanediyl-bis-phosphonic acid tetrachloride (1499-29-2) + 2-(4-nitrobenzylidene)propane-1,3-diol (104143-50-2) + diethylamine (109-89-7) → C19H31N3O6P2 (1346258-39-6)

Guidance literature:

P,P'-methanediyl-bis-phosphonic acid tetrachloride; diethylamine; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;

2-(4-nitrobenzylidene)propane-1,3-diol; With dmap; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;

Reference yield:

4-nitrobenzyl chloride (100-14-1) → C19H31N3O6P2 (1346258-39-6)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium methylate / methanol / 24 h / Irradiation

2.1: Dowex / methanol / 24 h / Reflux

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

3.2: 2 h / 20 °C / Inert atmosphere

With sodium methylate; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane;

Reference yield:

2,2-dimethyl 5-p-nitrobenzylidene 1,3-dioxane (104143-49-9) → C19H31N3O6P2 (1346258-39-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: Dowex / methanol / 24 h / Reflux

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

2.2: 2 h / 20 °C / Inert atmosphere

With N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane;

upstream raw materials:

P,P'-methanediyl-bis-phosphonic acid tetrachloride

2-(4-nitrobenzylidene)propane-1,3-diol

diethylamine

4-nitrobenzyl chloride