ethyl (2E)-3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}prop-2-enoate

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Chemical Name:ethyl (2E)-3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}prop-2-enoate
CAS No.:1356602-51-1
Molecular Formula:C₂₇H₂₇NO₅
Molecular Weight:445.515
Hs Code.:

Synonyms:ethyl (2E)-3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}prop-2-enoate

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Chemical Property of ethyl (2E)-3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}prop-2-enoate

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Technology Process of ethyl (2E)-3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}prop-2-enoate

There total 3 articles about ethyl (2E)-3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}prop-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 70-11-1
α-bromoacetophenone

: 1356602-51-1
ethyl (2E)-3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}prop-2-enoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium acetate; acetic acid / 0.08 h / 20 °C

1.2: 3 h / 20 - 80 °C

2.1: potassium carbonate / acetonitrile / 0.08 h / 20 °C

2.2: 5 h / 20 - 80 °C

3.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 12 h / 0 - 20 °C

4.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C

4.2: 12 h / 0 - 20 °C

With di-isopropyl azodicarboxylate; sodium acetate; sodium hydride; potassium carbonate; acetic acid; triphenylphosphine; In tetrahydrofuran; acetonitrile;

Reference yield:

: 142533-52-6
(Z)-2-bromo-1-phenylethanone O-methyl oxime

: 1356602-51-1
ethyl (2E)-3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}prop-2-enoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetonitrile / 0.08 h / 20 °C

1.2: 5 h / 20 - 80 °C

2.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 12 h / 0 - 20 °C

3.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C

3.2: 12 h / 0 - 20 °C

With di-isopropyl azodicarboxylate; sodium hydride; potassium carbonate; triphenylphosphine; In tetrahydrofuran; acetonitrile;

Reference yield:

: 1356599-86-4
(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}phenyl)methanol

: 1356602-51-1
ethyl (2E)-3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}prop-2-enoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 12 h / 0 - 20 °C

2.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C

2.2: 12 h / 0 - 20 °C

With di-isopropyl azodicarboxylate; sodium hydride; triphenylphosphine; In tetrahydrofuran;