Benzyl bis(2-bromoethyl)carbamate

Base Information

Chemical Name:Benzyl bis(2-bromoethyl)carbamate
CAS No.:189323-09-9
Molecular Formula:C12H15 Br2 N O2
Molecular Weight:365.065
Hs Code.:
European Community (EC) Number:881-483-2
DSSTox Substance ID:DTXSID60596590
Nikkaji Number:J3.339.983I
Wikidata:Q82491887
Mol file:189323-09-9.mol

Synonyms:189323-09-9;N-Cbz-N,N-bis(2-bromoethyl)amine;2-Bromo-N-(2-bromoethyl)-N-Cbz-ethanamine;BENZYL BIS(2-BROMOETHYL)CARBAMATE;BENZYL N,N-BIS(2-BROMOETHYL)CARBAMATE;MFCD11519273;Carbamic acid, N,N-bis(2-bromoethyl)-, phenylmethyl ester;SCHEMBL264989;DTXSID60596590;KZXFVMMTKPFXAO-UHFFFAOYSA-N;AKOS015909144;AS-40526;SY027319;A4182;CS-0197829;N-Benzyloxycarbonyl-N,N-bis(2-bromoethyl)amine;2-CHLORO-5-[(ISOPROPYLAMINO)SULFONYL]BENZOICACID

Suppliers and Price of Benzyl bis(2-bromoethyl)carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Labseeker
benzylbis(2-bromoethyl)carbamate 95
10g
$ 1467.00

Crysdot
2-Bromo-N-(2-bromoethyl)-N-Cbz-ethanamine 95+%
5g
$ 465.00

Chemenu
benzylN,N-bis(2-bromoethyl)carbamate 95%+
100g
$ 3327.00

Chemenu
benzylN,N-bis(2-bromoethyl)carbamate 95%+
25g
$ 2038.00

American Custom Chemicals Corporation
BENZYL BIS(2-BROMOETHYL)CARBAMATE 95.00%
5MG
$ 501.26

AK Scientific
N-Cbz-N,N-bis(2-bromoethyl)amine
1g
$ 297.00

Acrotein
2-Bromo-N-(2-bromoethyl)-N-Cbz-ethanamine 97%
10g
$ 495.00

Acrotein
2-Bromo-N-(2-bromoethyl)-N-Cbz-ethanamine 97%
5g
$ 330.00

Total 9 raw suppliers

Chemical Property of Benzyl bis(2-bromoethyl)carbamate

Chemical Property:

Boiling Point:402.3±45.0 °C(Predicted)
PKA:-1.85±0.70(Predicted)
PSA：29.54000
Density:1.619±0.06 g/cm3(Predicted)
LogP:3.41500
XLogP3:3.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:7
Exact Mass:364.94490
Heavy Atom Count:17
Complexity:215

Purity/Quality:

97% ^*data from raw suppliers

benzylbis(2-bromoethyl)carbamate 95 ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)COC(=O)N(CCBr)CCBr

Technology Process of Benzyl bis(2-bromoethyl)carbamate

There total 3 articles about Benzyl bis(2-bromoethyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 43204-63-3
bis(2-bromoethyl)amine hydrobromide

: 501-53-1,94274-21-2
benzyl chloroformate

: 189323-09-9
benzyl bis(2-bromoethyl)carbamate

Guidance literature:: With sodium hydroxide; at 0 ℃;
DOI:10.1016/S0960-894X(97)00213-8

Reference yield: 70.0%

: 70782-12-6
N-benzyloxycarbonyldiethanolamine

: 189323-09-9
benzyl bis(2-bromoethyl)carbamate

Guidance literature:: With 1H-imidazole; bromine; triphenylphosphine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol502207z

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 189323-09-9
benzyl bis(2-bromoethyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / water / 24 h / 20 °C

2: carbon tetrabromide; triphenylphosphine / dichloromethane / 5 h / 20 °C

With carbon tetrabromide; sodium hydrogencarbonate; triphenylphosphine; In dichloromethane; water;