C₃₀H₃₂N₄O₂*C₂₉H₄₄N₂O

Base Information

• Chemical Name: C₃₀H₃₂N₄O₂*C₂₉H₄₄N₂O
• CAS No.: 1609137-36-1
• Molecular Formula: C₂₉H₄₄N₂O*C₃₀H₃₂N₄O₂
• Molecular Weight: 917.291
• Mol file: 1609137-36-1.mol

Synonyms:C₃₀H₃₂N₄O₂*C₂₉H₄₄N₂O

Chemical Property of C₃₀H₃₂N₄O₂*C₂₉H₄₄N₂O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₃₂N₄O₂*C₂₉H₄₄N₂O

There total 4 articles about C₃₀H₃₂N₄O₂*C₂₉H₄₄N₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

2,6-Pyridinedicarboxaldehyde (5431-44-7) + C23H27N3O2 (1609137-34-9) + 1,3-bis(3,5-di-tert-butylphenyl)urea (16225-25-5) → C30H32N4O2*C29H44N2O (1609137-36-1)

Guidance literature:

2,6-Pyridinedicarboxaldehyde; C₂₃H₂₇N₃O₂; 1,3-bis(3,5-di-tert-butylphenyl)urea; With sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate; In chloroform; at 50 ℃; for 43h;

With sodium tetrahydroborate; In methanol; chloroform; at 20 ℃;

DOI:10.1002/chem.201400323

Reference yield:

2.6-bis(hydroxymethyl)pyridine (1195-59-1) → C30H32N4O2*C29H44N2O (1609137-36-1)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h / Reflux

1.2: 16 h / Reflux

2.1: borane-THF / tetrahydrofuran / 16 h / Reflux

3.1: sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate / chloroform / 43 h / 50 °C

3.2: 20 °C

With borane-THF; sodium hydride; sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate; In tetrahydrofuran; chloroform;

DOI:10.1002/chem.201400323

Reference yield:

4-cyanobenzyl bromide (17201-43-3) → C30H32N4O2*C29H44N2O (1609137-36-1)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h / Reflux

1.2: 16 h / Reflux

2.1: borane-THF / tetrahydrofuran / 16 h / Reflux

3.1: sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate / chloroform / 43 h / 50 °C

3.2: 20 °C

With borane-THF; sodium hydride; sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate; In tetrahydrofuran; chloroform;

DOI:10.1002/chem.201400323

upstream raw materials:

4,4'-(((pyridine-2,6-diylbis(methylene))bis(oxy))bis(methylene))dibenzonitrile

2.6-bis(hydroxymethyl)pyridine

4-cyanobenzyl bromide

2,6-Pyridinedicarboxaldehyde