dibenzylmalonyl Dichloride

Base Information

Chemical Name:dibenzylmalonyl Dichloride
CAS No.:40932-28-3
Molecular Formula:C₁₇H₁₄Cl₂O₂
Molecular Weight:321.203
Hs Code.:

Synonyms:dibenzylmalonyl Dichloride

Suppliers and Price of dibenzylmalonyl Dichloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dibenzylmalonyl Dichloride

Chemical Property:

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Technology Process of dibenzylmalonyl Dichloride

There total 8 articles about dibenzylmalonyl Dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 4372-32-1
dibenzylmalonic acid

: 40932-28-3
dibenzylmalonyl Dichloride

Guidance literature:: In thionyl chloride;

Reference yield:

: 597-55-7
dibenzylmalonic acid diethyl ester

: 40932-28-3
dibenzylmalonyl Dichloride

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / sodium hydroxide / ethanol; H₂O / 6 h / 90 °C

2: 72 percent / phosphorus pentachloride / CHCl₃ / 0.25 h / Heating

With sodium hydroxide; phosphorus pentachloride; In ethanol; chloroform; water; 1: Hydrolysis / 2: Substitution;
DOI:10.1021/jo990867j

Reference yield:

: 100-44-7
benzyl chloride

: 40932-28-3
dibenzylmalonyl Dichloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium ethoxide / ethanol / 0.5 h

1.2: 98 percent / ethanol / 0 - 25 °C

2.1: 85 percent / sodium hydroxide / ethanol; H₂O / 6 h / 90 °C

3.1: 72 percent / phosphorus pentachloride / CHCl₃ / 0.25 h / Heating

With sodium hydroxide; phosphorus pentachloride; sodium ethanolate; In ethanol; chloroform; water; 1.1: Metallation / 1.2: Alkylation / 2.1: Hydrolysis / 3.1: Substitution;
DOI:10.1021/jo990867j