35-benzylthio-1-(N-phthalimido)-3,6,9,12,15,18,21,24,27,30,33-undecaoxapentatriacontane

Base Information

Chemical Name:35-benzylthio-1-(N-phthalimido)-3,6,9,12,15,18,21,24,27,30,33-undecaoxapentatriacontane
CAS No.:194425-36-0
Molecular Formula:C₃₉H₅₉NO₁₃S
Molecular Weight:781.962
Hs Code.:

Synonyms:35-benzylthio-1-(N-phthalimido)-3,6,9,12,15,18,21,24,27,30,33-undecaoxapentatriacontane

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Chemical Property of 35-benzylthio-1-(N-phthalimido)-3,6,9,12,15,18,21,24,27,30,33-undecaoxapentatriacontane

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Technology Process of 35-benzylthio-1-(N-phthalimido)-3,6,9,12,15,18,21,24,27,30,33-undecaoxapentatriacontane

There total 12 articles about 35-benzylthio-1-(N-phthalimido)-3,6,9,12,15,18,21,24,27,30,33-undecaoxapentatriacontane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1074-82-4
potassium phtalimide

: 194425-34-8
35-benzylthio-3,6,9,12,15,18,21,24,27,30,33-undecaoxapentatriacontanyl chloride

: 194425-36-0
35-benzylthio-1-(N-phthalimido)-3,6,9,12,15,18,21,24,27,30,33-undecaoxapentatriacontane

Guidance literature:: In N,N-dimethyl-formamide; at 100 ℃;
DOI:10.1016/S0040-4020(97)00698-4

Reference yield:

: 42607-87-4
17-(2H-tetrahydropyran-2'-yloxy)-3,6,9,12,15-pentaoxaheptadecan-1-ol

: 194425-36-0
35-benzylthio-1-(N-phthalimido)-3,6,9,12,15,18,21,24,27,30,33-undecaoxapentatriacontane

Guidance literature:: Multi-step reaction with 5 steps

1: 33 percent / thionyl chloride, pyridine / CH₂Cl₂ / 18 h / Heating

2: 51 percent / aq. NaOH, tetrabutylammonium hydrogen sulfate / 72 h / 65 °C

3: 86 percent / 10-camphor sulfonic acid / methanol

4: 50 percent / thionyl chloride, pyridine / CH₂Cl₂ / 18 h / Heating

5: 51 percent / dimethylformamide / 100 °C

With pyridine; sodium hydroxide; thionyl chloride; camphor-10-sulfonic acid; tetra(n-butyl)ammonium hydrogensulfate; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(97)00698-4

Reference yield:

: 2615-15-8
pentaethylene glycol

: 194425-36-0
35-benzylthio-1-(N-phthalimido)-3,6,9,12,15,18,21,24,27,30,33-undecaoxapentatriacontane

Guidance literature:: Multi-step reaction with 6 steps

1: 34 percent / conc. HCl / 12 h / Ambient temperature

2: 33 percent / thionyl chloride, pyridine / CH₂Cl₂ / 18 h / Heating

3: 51 percent / aq. NaOH, tetrabutylammonium hydrogen sulfate / 72 h / 65 °C

4: 86 percent / 10-camphor sulfonic acid / methanol

5: 50 percent / thionyl chloride, pyridine / CH₂Cl₂ / 18 h / Heating

6: 51 percent / dimethylformamide / 100 °C

With pyridine; hydrogenchloride; sodium hydroxide; thionyl chloride; camphor-10-sulfonic acid; tetra(n-butyl)ammonium hydrogensulfate; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(97)00698-4