5,8,11,14,17,20,23,26,29,32,35-Undecaoxa-2-thiaheptatriacontane, 37-chloro-1-phenyl-

Base Information

Chemical Name:5,8,11,14,17,20,23,26,29,32,35-Undecaoxa-2-thiaheptatriacontane, 37-chloro-1-phenyl-
CAS No.:194425-34-8
Molecular Formula:C₃₁H₅₅ClO₁₁S
Molecular Weight:671.29
Hs Code.:
Mol file:194425-34-8.mol

Synonyms:

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Chemical Property of 5,8,11,14,17,20,23,26,29,32,35-Undecaoxa-2-thiaheptatriacontane, 37-chloro-1-phenyl-

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Technology Process of 5,8,11,14,17,20,23,26,29,32,35-Undecaoxa-2-thiaheptatriacontane, 37-chloro-1-phenyl-

There total 10 articles about 5,8,11,14,17,20,23,26,29,32,35-Undecaoxa-2-thiaheptatriacontane, 37-chloro-1-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 42607-87-4
17-(2H-tetrahydropyran-2'-yloxy)-3,6,9,12,15-pentaoxaheptadecan-1-ol

: 194425-34-8
35-benzylthio-3,6,9,12,15,18,21,24,27,30,33-undecaoxapentatriacontanyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: 33 percent / thionyl chloride, pyridine / CH₂Cl₂ / 18 h / Heating

2: 51 percent / aq. NaOH, tetrabutylammonium hydrogen sulfate / 72 h / 65 °C

3: 86 percent / 10-camphor sulfonic acid / methanol

4: 50 percent / thionyl chloride, pyridine / CH₂Cl₂ / 18 h / Heating

With pyridine; sodium hydroxide; thionyl chloride; camphor-10-sulfonic acid; tetra(n-butyl)ammonium hydrogensulfate; In methanol; dichloromethane;
DOI:10.1016/S0040-4020(97)00698-4

Reference yield:

: 2615-15-8
pentaethylene glycol

: 194425-34-8
35-benzylthio-3,6,9,12,15,18,21,24,27,30,33-undecaoxapentatriacontanyl chloride

Guidance literature:: Multi-step reaction with 5 steps

1: 34 percent / conc. HCl / 12 h / Ambient temperature

2: 33 percent / thionyl chloride, pyridine / CH₂Cl₂ / 18 h / Heating

3: 51 percent / aq. NaOH, tetrabutylammonium hydrogen sulfate / 72 h / 65 °C

4: 86 percent / 10-camphor sulfonic acid / methanol

5: 50 percent / thionyl chloride, pyridine / CH₂Cl₂ / 18 h / Heating

With pyridine; hydrogenchloride; sodium hydroxide; thionyl chloride; camphor-10-sulfonic acid; tetra(n-butyl)ammonium hydrogensulfate; In methanol; dichloromethane;
DOI:10.1016/S0040-4020(97)00698-4

Reference yield:

: 5197-62-6
2-[2-(chloroethoxy)ethoxy]ethanol

: 194425-34-8
35-benzylthio-3,6,9,12,15,18,21,24,27,30,33-undecaoxapentatriacontanyl chloride

Guidance literature:: Multi-step reaction with 6 steps

1: 78 percent / sodium / ethanol / Heating

2: aq. NaOH, tetrabutylammonium hydrogensulfate / CH₂Cl₂ / 72 h / 65 °C

3: 10-camphorsulfonic acid / methanol

4: 51 percent / aq. NaOH, tetrabutylammonium hydrogen sulfate / 72 h / 65 °C

5: 86 percent / 10-camphor sulfonic acid / methanol

6: 50 percent / thionyl chloride, pyridine / CH₂Cl₂ / 18 h / Heating

With pyridine; sodium hydroxide; thionyl chloride; camphor-10-sulfonic acid; (1S)-10-camphorsulfonic acid; tetra(n-butyl)ammonium hydrogensulfate; sodium; In methanol; ethanol; dichloromethane;
DOI:10.1016/S0040-4020(97)00698-4