N-(4-(9H-carbazol-9-yl)phenyl)-4-bromo-N-(4-bromophenyl)aniline

Base Information

• Chemical Name: N-(4-(9H-carbazol-9-yl)phenyl)-4-bromo-N-(4-bromophenyl)aniline
• CAS No.: 1219104-72-9
• Molecular Formula: C₃₀H₂₀Br₂N₂
• Molecular Weight: 568.31
• Mol file: 1219104-72-9.mol

Synonyms:N-(4-(9H-carbazol-9-yl)phenyl)-4-bromo-N-(4-bromophenyl)aniline

Chemical Property of N-(4-(9H-carbazol-9-yl)phenyl)-4-bromo-N-(4-bromophenyl)aniline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of N-(4-(9H-carbazol-9-yl)phenyl)-4-bromo-N-(4-bromophenyl)aniline

There total 3 articles about N-(4-(9H-carbazol-9-yl)phenyl)-4-bromo-N-(4-bromophenyl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

tri(p-bromophenyl)amine (4316-58-9) + 9H-carbazole (86-74-8,105184-46-1,97960-57-1) → N-(4-(9H-carbazol-9-yl)phenyl)-4-bromo-N-(4-bromophenyl)aniline (1219104-72-9) + N-(4-(9H-carbazol-9-yl)phenyl)-N-(4-bromophenyl)-4-(9Hcarbazol-9-yl)-benzenamine (1392844-97-1) + 4,4',4-tris(N-carbazolyl)triphenylamine

Guidance literature:

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; copper(l) iodide; 18-crown-6 ether; potassium carbonate; for 48h; Reflux; Inert atmosphere;

DOI:10.1039/c4tc00951g

Reference yield: 16.3%

1,4-bromoiodobenzene (589-87-7) + 4-(9H-carbazol-9-yl)aniline (52708-37-9) → N-(4-(9H-carbazol-9-yl)phenyl)-4-bromo-N-(4-bromophenyl)aniline (1219104-72-9)

Guidance literature:

With sodium t-butanolate; 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; In toluene; for 24h; Inert atmosphere; Reflux;

Reference yield:

tri(p-bromophenyl)amine (4316-58-9) + 9H-carbazole (86-74-8,105184-46-1,97960-57-1) → N-(4-(9H-carbazol-9-yl)phenyl)-4-bromo-N-(4-bromophenyl)aniline (1219104-72-9)

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; sodium t-butanolate; In tetrahydrofuran;

DOI:10.1166/jnn.2019.16688

upstream raw materials:

1,4-bromoiodobenzene

4-(9H-carbazol-9-yl)aniline

tri(p-bromophenyl)amine

9H-carbazole