((2-(<3'-(1-thio-(phenylphosphino)phenyl)propyl>phenylphosphino)phenyl)thio)methyl methyl ether

Base Information

Chemical Name:((2-(<3'-(1-thio-(phenylphosphino)phenyl)propyl>phenylphosphino)phenyl)thio)methyl methyl ether
CAS No.:94890-98-9
Molecular Formula:C₂₉H₃₀OP₂S₂
Molecular Weight:520.636
Hs Code.:

Synonyms:((2-(<3'-(1-thio-(phenylphosphino)phenyl)propyl>phenylphosphino)phenyl)thio)methyl methyl ether

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Chemical Property of ((2-(<3'-(1-thio-(phenylphosphino)phenyl)propyl>phenylphosphino)phenyl)thio)methyl methyl ether

Chemical Property:

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Technology Process of ((2-(<3'-(1-thio-(phenylphosphino)phenyl)propyl>phenylphosphino)phenyl)thio)methyl methyl ether

There total 7 articles about ((2-(<3'-(1-thio-(phenylphosphino)phenyl)propyl>phenylphosphino)phenyl)thio)methyl methyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65000-89-7
Ethyl-(o-nitrophenyl)-phenylphosphinat

: 94890-98-9
((2-(<3'-(1-thio-(phenylphosphino)phenyl)propyl>phenylphosphino)phenyl)thio)methyl methyl ether

Guidance literature:: Multi-step reaction with 5 steps

1: Fe, NH₄Cl / H₂O / Heating

3: 76 percent

4: 96 percent / 2.64 M n-butyllithium / hexane; tetrahydrofuran / -78 °C

5: potassium hydroxide / tetrahydrofuran; aq. ethanol / 106 h / Ambient temperature

With potassium hydroxide; n-butyllithium; iron; ammonium chloride; In tetrahydrofuran; ethanol; hexane; water;
DOI:10.1021/ja00293a052

Reference yield:

: 1638-86-4
diethyl phenylphosphonite

: 94890-98-9
((2-(<3'-(1-thio-(phenylphosphino)phenyl)propyl>phenylphosphino)phenyl)thio)methyl methyl ether

Guidance literature:: Multi-step reaction with 6 steps

1: 25 °C

2: Fe, NH₄Cl / H₂O / Heating

4: 76 percent

5: 96 percent / 2.64 M n-butyllithium / hexane; tetrahydrofuran / -78 °C

6: potassium hydroxide / tetrahydrofuran; aq. ethanol / 106 h / Ambient temperature

With potassium hydroxide; n-butyllithium; iron; ammonium chloride; In tetrahydrofuran; ethanol; hexane; water;
DOI:10.1021/ja00293a052

Reference yield:

: 528-29-0
1,2-Dinitrobenzene

: 94890-98-9
((2-(<3'-(1-thio-(phenylphosphino)phenyl)propyl>phenylphosphino)phenyl)thio)methyl methyl ether

Guidance literature:: Multi-step reaction with 6 steps

1: 25 °C

2: Fe, NH₄Cl / H₂O / Heating

4: 76 percent

5: 96 percent / 2.64 M n-butyllithium / hexane; tetrahydrofuran / -78 °C

6: potassium hydroxide / tetrahydrofuran; aq. ethanol / 106 h / Ambient temperature

With potassium hydroxide; n-butyllithium; iron; ammonium chloride; In tetrahydrofuran; ethanol; hexane; water;
DOI:10.1021/ja00293a052