benzyl 4-methoxy-3-(N-(2-(4-methylpiperazin-1-yl)-2-oxoethyl)methylsulfonamido)benzoate

Base Information

Chemical Name:benzyl 4-methoxy-3-(N-(2-(4-methylpiperazin-1-yl)-2-oxoethyl)methylsulfonamido)benzoate
CAS No.:1610862-15-1
Molecular Formula:C₂₃H₂₉N₃O₆S
Molecular Weight:475.566
Hs Code.:

Synonyms:benzyl 4-methoxy-3-(N-(2-(4-methylpiperazin-1-yl)-2-oxoethyl)methylsulfonamido)benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 4-methoxy-3-(N-(2-(4-methylpiperazin-1-yl)-2-oxoethyl)methylsulfonamido)benzoate

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Technology Process of benzyl 4-methoxy-3-(N-(2-(4-methylpiperazin-1-yl)-2-oxoethyl)methylsulfonamido)benzoate

There total 5 articles about benzyl 4-methoxy-3-(N-(2-(4-methylpiperazin-1-yl)-2-oxoethyl)methylsulfonamido)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1428847-58-8
benzyl 4-methoxy-3-(methylsulfonamido)benzoate

: 42951-91-7
2-chloro-1-(4-methylpiperazin-1-yl)ethan-1-one hydrochloride

: 1610862-15-1
benzyl 4-methoxy-3-(N-(2-(4-methylpiperazin-1-yl)-2-oxoethyl)methylsulfonamido)benzoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 70 ℃; for 1h;

Reference yield:

: 100-39-0
benzyl bromide

: 1610862-15-1
benzyl 4-methoxy-3-(N-(2-(4-methylpiperazin-1-yl)-2-oxoethyl)methylsulfonamido)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

1.2: 8 h / 20 °C

2.1: ammonium chloride; iron / water; ethanol / 2 h / 80 °C

3.1: pyridine / 0 - 20 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 70 °C

With pyridine; iron; potassium carbonate; ammonium chloride; caesium carbonate; In ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: benzyl 4-methoxy-3-nitrobenzoate

: 1610862-15-1
benzyl 4-methoxy-3-(N-(2-(4-methylpiperazin-1-yl)-2-oxoethyl)methylsulfonamido)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium chloride; iron / water; ethanol / 2 h / 80 °C

2: pyridine / 0 - 20 °C

3: potassium carbonate / N,N-dimethyl-formamide / 1 h / 70 °C

With pyridine; iron; potassium carbonate; ammonium chloride; In ethanol; water; N,N-dimethyl-formamide;