4-biphenylyl triphenylphosphinegold(I)

Base Information

Chemical Name:4-biphenylyl triphenylphosphinegold(I)
CAS No.:934282-52-7
Molecular Formula:C₃₀H₂₄AuP
Molecular Weight:612.461
Hs Code.:

Synonyms:4-biphenylyl triphenylphosphinegold(I)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-biphenylyl triphenylphosphinegold(I)

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Technology Process of 4-biphenylyl triphenylphosphinegold(I)

There total 1 articles about 4-biphenylyl triphenylphosphinegold(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 14243-64-2
(triphenylphosphine)gold(I) chloride

: 92-66-0
4-bromo-1,1'-biphenyl

: 934282-52-7
4-biphenylyl triphenylphosphinegold(I)

Guidance literature:: In tetrahydrofuran; hexane; under Ar, 1.60 M soln. of n-BuLi in hexane was added to THF soln. of Br-compd. at -70 °C, Au-compd. was added after 10 min, stirring at -70 °C for 30 min, mixt. was allowed to warm to room temp.; solvent was removed in vac., recrystn. from Et2O soln., elem. anal.;
DOI:10.1016/j.cplett.2007.01.002

Reference yield: 75.0%

: 75-09-2
dichloromethane

: 934282-52-7
4-biphenylyl triphenylphosphinegold(I)

: 14243-64-2
(triphenylphosphine)gold(I) chloride

Guidance literature:: In dichloromethane; byproducts: biphenyl; Irradiation (UV/VIS); under Ar, laser irradn. at 266 nm; monitored by UV and emission spectroscopy;
DOI:10.1016/j.cplett.2007.01.002

Reference yield:

: 1665-00-5
dichloromethane-d2

: 934282-52-7
4-biphenylyl triphenylphosphinegold(I)

: 14243-64-2
(triphenylphosphine)gold(I) chloride

Guidance literature:: In dichloromethane; byproducts: 4-deuterobiphenyl; Irradiation (UV/VIS); under Ar, laser irradn. at 266 nm; monitored by UV and emission spectroscopy;
DOI:10.1016/j.cplett.2007.01.002