(S)-4-(1-benzyl-3-methyl-1H-pyrazol-5-yl)-N-(N,N-dimethylsulfamoyl)-1-(2,2-diphenylacetyl)piperazine-2-carboxamide

Base Information

Chemical Name:(S)-4-(1-benzyl-3-methyl-1H-pyrazol-5-yl)-N-(N,N-dimethylsulfamoyl)-1-(2,2-diphenylacetyl)piperazine-2-carboxamide
CAS No.:1448679-01-3
Molecular Formula:C₃₂H₃₆N₆O₄S
Molecular Weight:600.742
Hs Code.:

Synonyms:(S)-4-(1-benzyl-3-methyl-1H-pyrazol-5-yl)-N-(N,N-dimethylsulfamoyl)-1-(2,2-diphenylacetyl)piperazine-2-carboxamide

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Chemical Property of (S)-4-(1-benzyl-3-methyl-1H-pyrazol-5-yl)-N-(N,N-dimethylsulfamoyl)-1-(2,2-diphenylacetyl)piperazine-2-carboxamide

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Technology Process of (S)-4-(1-benzyl-3-methyl-1H-pyrazol-5-yl)-N-(N,N-dimethylsulfamoyl)-1-(2,2-diphenylacetyl)piperazine-2-carboxamide

There total 12 articles about (S)-4-(1-benzyl-3-methyl-1H-pyrazol-5-yl)-N-(N,N-dimethylsulfamoyl)-1-(2,2-diphenylacetyl)piperazine-2-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 3984-14-3
N,N-dimethylsulfamide

: 1448678-93-0
(S)-4-(1-benzyl-3-methyl-1H-pyrazol-5-yl)-1-(2,2-diphenylacetyl)piperazine-2-carboxylic acid

: 1448679-01-3
(S)-4-(1-benzyl-3-methyl-1H-pyrazol-5-yl)-N-(N,N-dimethylsulfamoyl)-1-(2,2-diphenylacetyl)piperazine-2-carboxamide

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃;

Reference yield:

: 796096-64-5
(S)-piperazine-1,2-dicarboxylic acid 1-tert-butyl ester 2-methyl ester

: 1448679-01-3
(S)-4-(1-benzyl-3-methyl-1H-pyrazol-5-yl)-N-(N,N-dimethylsulfamoyl)-1-(2,2-diphenylacetyl)piperazine-2-carboxamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: toluene / 100 °C

2.1: Lawessons reagent / toluene / 75 °C

3.1: hydrazine hydrate / toluene / 70 °C

4.1: caesium carbonate / N,N-dimethyl-formamide / 45 °C

4.2: 3 h / 20 °C

5.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 20 °C

With Lawessons reagent; dmap; caesium carbonate; hydrazine hydrate; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1448679-11-5
C₁₅H₂₄N₂O₆

: 1448679-01-3
(S)-4-(1-benzyl-3-methyl-1H-pyrazol-5-yl)-N-(N,N-dimethylsulfamoyl)-1-(2,2-diphenylacetyl)piperazine-2-carboxamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: Lawessons reagent / toluene / 75 °C

2.1: hydrazine hydrate / toluene / 70 °C

3.1: caesium carbonate / N,N-dimethyl-formamide / 45 °C

3.2: 3 h / 20 °C

4.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 20 °C

With Lawessons reagent; dmap; caesium carbonate; hydrazine hydrate; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide; toluene;