2,6-dihydroxymethyl-3,5-bis(2,5,8,11-tetraoxadodecyl)phenyl methoxymethyl ether

Base Information

Chemical Name:2,6-dihydroxymethyl-3,5-bis(2,5,8,11-tetraoxadodecyl)phenyl methoxymethyl ether
CAS No.:1333471-48-9
Molecular Formula:C₂₆H₄₆O₁₂
Molecular Weight:550.644
Hs Code.:

Synonyms:2,6-dihydroxymethyl-3,5-bis(2,5,8,11-tetraoxadodecyl)phenyl methoxymethyl ether

Suppliers and Price of 2,6-dihydroxymethyl-3,5-bis(2,5,8,11-tetraoxadodecyl)phenyl methoxymethyl ether

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,6-dihydroxymethyl-3,5-bis(2,5,8,11-tetraoxadodecyl)phenyl methoxymethyl ether

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,6-dihydroxymethyl-3,5-bis(2,5,8,11-tetraoxadodecyl)phenyl methoxymethyl ether

There total 4 articles about 2,6-dihydroxymethyl-3,5-bis(2,5,8,11-tetraoxadodecyl)phenyl methoxymethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1333471-46-7
2-methoxymethoxy-4,6-bis(2,5,8,11-tetraoxadodecyl)isophthalic acid dimethyl ester

: 1333471-48-9
2,6-dihydroxymethyl-3,5-bis(2,5,8,11-tetraoxadodecyl)phenyl methoxymethyl ether

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 25 ℃; Inert atmosphere;
DOI:10.1039/c1dt10556f

Reference yield:

: 1333471-42-3
4,6-dimethyl-2-methoxymethoxyisophthalic acid dimethyl ester

: 1333471-48-9
2,6-dihydroxymethyl-3,5-bis(2,5,8,11-tetraoxadodecyl)phenyl methoxymethyl ether

Guidance literature:: Multi-step reaction with 3 steps

1.1: 2,2'-azobis(isobutyronitrile) / dichloromethane / 1 h / 25 °C / Inert atmosphere; Irradiation

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere

2.2: 0 °C / Inert atmosphere

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 25 °C / Inert atmosphere

With lithium aluminium tetrahydride; 2,2'-azobis(isobutyronitrile); sodium hydride; In tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1039/c1dt10556f

Reference yield:

: 76716-11-5
1,3-benzenedicarboxylic acid 2-hydroxy-4,6-dimethyl-1,3-dimethyl ester

: 1333471-48-9
2,6-dihydroxymethyl-3,5-bis(2,5,8,11-tetraoxadodecyl)phenyl methoxymethyl ether

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C / Inert atmosphere

1.2: 0 - 25 °C / Inert atmosphere

2.1: 2,2'-azobis(isobutyronitrile) / dichloromethane / 1 h / 25 °C / Inert atmosphere; Irradiation

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere

3.2: 0 °C / Inert atmosphere

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 25 °C / Inert atmosphere

With lithium aluminium tetrahydride; 2,2'-azobis(isobutyronitrile); sodium hydride; In tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1039/c1dt10556f