2-methoxymethoxy-4,6-bis(2,5,8,11-tetraoxadodecyl)isophthalic acid dimethyl ester

Base Information

Chemical Name:2-methoxymethoxy-4,6-bis(2,5,8,11-tetraoxadodecyl)isophthalic acid dimethyl ester
CAS No.:1333471-46-7
Molecular Formula:C₂₈H₄₆O₁₄
Molecular Weight:606.665
Hs Code.:

Synonyms:2-methoxymethoxy-4,6-bis(2,5,8,11-tetraoxadodecyl)isophthalic acid dimethyl ester

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Chemical Property of 2-methoxymethoxy-4,6-bis(2,5,8,11-tetraoxadodecyl)isophthalic acid dimethyl ester

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Technology Process of 2-methoxymethoxy-4,6-bis(2,5,8,11-tetraoxadodecyl)isophthalic acid dimethyl ester

There total 3 articles about 2-methoxymethoxy-4,6-bis(2,5,8,11-tetraoxadodecyl)isophthalic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 112-35-6,95507-80-5
triethylene glucol monomethyl ether

: 1333471-44-5
4,6-bis(bromomethyl)-2-methoxymethoxyisophthalic acid dimethyl ester

: 1333471-46-7
2-methoxymethoxy-4,6-bis(2,5,8,11-tetraoxadodecyl)isophthalic acid dimethyl ester

Guidance literature:: triethylene glucol monomethyl ether; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.5h; Inert atmosphere;

4,6-bis(bromomethyl)-2-methoxymethoxyisophthalic acid dimethyl ester; In tetrahydrofuran; mineral oil; at 0 ℃; Inert atmosphere;
DOI:10.1039/c1dt10556f

Reference yield:

: 1333471-42-3
4,6-dimethyl-2-methoxymethoxyisophthalic acid dimethyl ester

: 1333471-46-7
2-methoxymethoxy-4,6-bis(2,5,8,11-tetraoxadodecyl)isophthalic acid dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 2,2'-azobis(isobutyronitrile) / dichloromethane / 1 h / 25 °C / Inert atmosphere; Irradiation

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere

2.2: 0 °C / Inert atmosphere

With 2,2'-azobis(isobutyronitrile); sodium hydride; In tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1039/c1dt10556f

Reference yield:

: 76716-11-5
1,3-benzenedicarboxylic acid 2-hydroxy-4,6-dimethyl-1,3-dimethyl ester

: 1333471-46-7
2-methoxymethoxy-4,6-bis(2,5,8,11-tetraoxadodecyl)isophthalic acid dimethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C / Inert atmosphere

1.2: 0 - 25 °C / Inert atmosphere

2.1: 2,2'-azobis(isobutyronitrile) / dichloromethane / 1 h / 25 °C / Inert atmosphere; Irradiation

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere

3.2: 0 °C / Inert atmosphere

With 2,2'-azobis(isobutyronitrile); sodium hydride; In tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1039/c1dt10556f