2-benzyloxy-4-[butyl[4-(tert-butyldiphenylsiloxy) butyl]amino]benzaldehyde

Base Information

Chemical Name:2-benzyloxy-4-[butyl[4-(tert-butyldiphenylsiloxy) butyl]amino]benzaldehyde
CAS No.:1267606-07-4
Molecular Formula:C₃₈H₄₇NO₃Si
Molecular Weight:593.882
Hs Code.:

Synonyms:2-benzyloxy-4-[butyl[4-(tert-butyldiphenylsiloxy) butyl]amino]benzaldehyde

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Chemical Property of 2-benzyloxy-4-[butyl[4-(tert-butyldiphenylsiloxy) butyl]amino]benzaldehyde

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Technology Process of 2-benzyloxy-4-[butyl[4-(tert-butyldiphenylsiloxy) butyl]amino]benzaldehyde

There total 6 articles about 2-benzyloxy-4-[butyl[4-(tert-butyldiphenylsiloxy) butyl]amino]benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.5%

: 1267606-06-3
2-benzyloxy-4-[butyl(4-hydroxybutyl)amino]benzaldehyde

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1267606-07-4
2-benzyloxy-4-[butyl[4-(tert-butyldiphenylsiloxy) butyl]amino]benzaldehyde

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

Reference yield:

: 4543-95-7
N-butyl-4-hydroxybutan-1-amine

: 1267606-07-4
2-benzyloxy-4-[butyl[4-(tert-butyldiphenylsiloxy) butyl]amino]benzaldehyde

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hexamethylsilazane / 1,4-dioxane / 22 h / 100 °C

2.1: 1 h / 80 °C

3.1: trichlorophosphate / 1.13 h / Cooling with ice

3.2: 1.5 h / 50 - 70 °C

4.1: sodium hydroxide; water / ethanol / 0.5 h / 20 °C

5.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 20 °C

With 1H-imidazole; water; potassium hexamethylsilazane; sodium hydroxide; trichlorophosphate; In 1,4-dioxane; ethanol; N,N-dimethyl-formamide;

Reference yield:

: 1267606-02-9
4-[(3-benzyloxyphenyl)butylamino]butyl acetate

: 1267606-07-4
2-benzyloxy-4-[butyl[4-(tert-butyldiphenylsiloxy) butyl]amino]benzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: trichlorophosphate / 1.13 h / Cooling with ice

1.2: 1.5 h / 50 - 70 °C

2.1: sodium hydroxide; water / ethanol / 0.5 h / 20 °C

3.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 20 °C

With 1H-imidazole; water; sodium hydroxide; trichlorophosphate; In ethanol; N,N-dimethyl-formamide;