[3-benzyloxy-4-(2-thiophene-2-ylvinyl)phenyl]butyl[4-(tert-butyldiphenylsiloxy) butyl]amine

Base Information

Chemical Name:[3-benzyloxy-4-(2-thiophene-2-ylvinyl)phenyl]butyl[4-(tert-butyldiphenylsiloxy) butyl]amine
CAS No.:1267606-10-9
Molecular Formula:C₄₃H₅₁NO₂SSi
Molecular Weight:674.035
Hs Code.:

Synonyms:[3-benzyloxy-4-(2-thiophene-2-ylvinyl)phenyl]butyl[4-(tert-butyldiphenylsiloxy) butyl]amine

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Chemical Property of [3-benzyloxy-4-(2-thiophene-2-ylvinyl)phenyl]butyl[4-(tert-butyldiphenylsiloxy) butyl]amine

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Technology Process of [3-benzyloxy-4-(2-thiophene-2-ylvinyl)phenyl]butyl[4-(tert-butyldiphenylsiloxy) butyl]amine

There total 7 articles about [3-benzyloxy-4-(2-thiophene-2-ylvinyl)phenyl]butyl[4-(tert-butyldiphenylsiloxy) butyl]amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.4%

: 1267606-07-4
2-benzyloxy-4-[butyl[4-(tert-butyldiphenylsiloxy) butyl]amino]benzaldehyde

: 3462-99-5
[(thien-2-yl)methyl]triphenylphosphonium chloride

: 1267606-10-9
[3-benzyloxy-4-(2-thiophene-2-ylvinyl)phenyl]butyl[4-(tert-butyldiphenylsiloxy) butyl]amine

Guidance literature:: [(thien-2-yl)methyl]triphenylphosphonium chloride; With phenyllithium; In tetrahydrofuran; dibutyl ether; for 0.25h; Cooling with ice; Inert atmosphere;

2-benzyloxy-4-[butyl[4-(tert-butyldiphenylsiloxy) butyl]amino]benzaldehyde; In tetrahydrofuran; dibutyl ether; for 2.13333h; Cooling with ice; Inert atmosphere;

Reference yield:

: 1267606-06-3
2-benzyloxy-4-[butyl(4-hydroxybutyl)amino]benzaldehyde

: 1267606-10-9
[3-benzyloxy-4-(2-thiophene-2-ylvinyl)phenyl]butyl[4-(tert-butyldiphenylsiloxy) butyl]amine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 20 °C

2.1: phenyllithium / dibutyl ether; tetrahydrofuran / 0.25 h / Cooling with ice; Inert atmosphere

2.2: 2.13 h / Cooling with ice; Inert atmosphere

With 1H-imidazole; phenyllithium; In tetrahydrofuran; dibutyl ether; N,N-dimethyl-formamide;

Reference yield:

: 1267606-02-9
4-[(3-benzyloxyphenyl)butylamino]butyl acetate

: 1267606-10-9
[3-benzyloxy-4-(2-thiophene-2-ylvinyl)phenyl]butyl[4-(tert-butyldiphenylsiloxy) butyl]amine

Guidance literature:: Multi-step reaction with 4 steps

1.1: trichlorophosphate / 1.13 h / Cooling with ice

1.2: 1.5 h / 50 - 70 °C

2.1: sodium hydroxide; water / ethanol / 0.5 h / 20 °C

3.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 20 °C

4.1: phenyllithium / dibutyl ether; tetrahydrofuran / 0.25 h / Cooling with ice; Inert atmosphere

4.2: 2.13 h / Cooling with ice; Inert atmosphere

With 1H-imidazole; water; phenyllithium; sodium hydroxide; trichlorophosphate; In tetrahydrofuran; ethanol; dibutyl ether; N,N-dimethyl-formamide;