N'-phenyl-hydrazinecarboxylic acid phenethyl ester

Base Information

Chemical Name:N'-phenyl-hydrazinecarboxylic acid phenethyl ester
CAS No.:40887-72-7
Molecular Formula:C₁₅H₁₆N₂O₂
Molecular Weight:256.304
Hs Code.:

Synonyms:N'-phenyl-hydrazinecarboxylic acid phenethyl ester

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Chemical Property of N'-phenyl-hydrazinecarboxylic acid phenethyl ester

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Technology Process of N'-phenyl-hydrazinecarboxylic acid phenethyl ester

There total 3 articles about N'-phenyl-hydrazinecarboxylic acid phenethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 124-38-9,18923-20-1
carbon dioxide

: 622-24-2
2-phenylethyl chloride

: 100-63-0
phenylhydrazine

: 40887-72-7
N'-phenyl-hydrazinecarboxylic acid phenethyl ester

Guidance literature:: carbon dioxide; phenylhydrazine; In dimethyl sulfoxide; at 60 ℃; for 0.5h; Inert atmosphere;

With N-benzyl-trimethylammonium hydroxide; In dimethyl sulfoxide; at 60 ℃; for 0.5h; Inert atmosphere;

2-phenylethyl chloride; In dimethyl sulfoxide; at 60 ℃; Inert atmosphere;
DOI:10.1007/s00706-008-0955-8

Reference yield: 87.0%

: 124-38-9,18923-20-1
carbon dioxide

: 4455-09-8
2-phenylethyl tosylate

: 100-63-0
phenylhydrazine

: 40887-72-7
N'-phenyl-hydrazinecarboxylic acid phenethyl ester

Guidance literature:: carbon dioxide; phenylhydrazine; With N-benzyl-trimethylammonium hydroxide; In dimethyl sulfoxide; at 60 ℃; for 0.5h; Inert atmosphere;

2-phenylethyl tosylate; In dimethyl sulfoxide; at 60 ℃; for 4h; Inert atmosphere;
DOI:10.1080/00397910802269259

Reference yield: 86.0%

: 124-38-9,18923-20-1
carbon dioxide

: 60-12-8
2-phenylethanol

: 100-63-0
phenylhydrazine

: 40887-72-7
N'-phenyl-hydrazinecarboxylic acid phenethyl ester

Guidance literature:: carbon dioxide; phenylhydrazine; In dimethyl sulfoxide; at 20 ℃; for 0.5h; Inert atmosphere;

2-phenylethanol; With triphenylphosphine; diethylazodicarboxylate; In dimethyl sulfoxide; at 20 ℃; for 3h; chemoselective reaction; Inert atmosphere;
DOI:10.1007/BF03249073