N-(2-(piperidin-4-yloxy)phenyl)pyridine-2-sulfonamide trifluoroacetate

Base Information

Chemical Name:N-(2-(piperidin-4-yloxy)phenyl)pyridine-2-sulfonamide trifluoroacetate
CAS No.:1378110-13-4
Molecular Formula:C₂₁H₂₇N₃O₅S
Molecular Weight:433.528
Hs Code.:

Synonyms:N-(2-(piperidin-4-yloxy)phenyl)pyridine-2-sulfonamide trifluoroacetate

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Chemical Property of N-(2-(piperidin-4-yloxy)phenyl)pyridine-2-sulfonamide trifluoroacetate

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Technology Process of N-(2-(piperidin-4-yloxy)phenyl)pyridine-2-sulfonamide trifluoroacetate

There total 4 articles about N-(2-(piperidin-4-yloxy)phenyl)pyridine-2-sulfonamide trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 66715-65-9
pyridine-2-sulfonyl chloride

: 690632-14-5
C₁₆H₂₄N₂O₃

: 1378110-13-4
N-(2-(piperidin-4-yloxy)phenyl)pyridine-2-sulfonamide trifluoroacetate

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 3h;

Reference yield:

: 88-75-5,78813-12-4
2-hydroxynitrobenzene

: 1378110-13-4
N-(2-(piperidin-4-yloxy)phenyl)pyridine-2-sulfonamide trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1: triphenylphosphine; diethylazodicarboxylate / 2 h / 20 °C

2: hydrogen / palladium on activated charcoal / methanol / 2 h / 20 °C / 3750.38 Torr

3: pyridine / dichloromethane / 3 h / 20 °C

With pyridine; hydrogen; triphenylphosphine; diethylazodicarboxylate; palladium on activated charcoal; In methanol; dichloromethane; 1: Mitsunobu reaction;

Reference yield:

: 109384-19-2
t-butyl 4-hydroxy piperidine-1-carboxylate

: 1378110-13-4
N-(2-(piperidin-4-yloxy)phenyl)pyridine-2-sulfonamide trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1: triphenylphosphine; diethylazodicarboxylate / 2 h / 20 °C

2: hydrogen / palladium on activated charcoal / methanol / 2 h / 20 °C / 3750.38 Torr

3: pyridine / dichloromethane / 3 h / 20 °C

With pyridine; hydrogen; triphenylphosphine; diethylazodicarboxylate; palladium on activated charcoal; In methanol; dichloromethane; 1: Mitsunobu reaction;