5-cyano-2-methylenepentanoic acid

Base Information

Chemical Name:5-cyano-2-methylenepentanoic acid
CAS No.:147766-06-1
Molecular Formula:C₇H₉NO₂
Molecular Weight:139.154
Hs Code.:

Synonyms:5-cyano-2-methylenepentanoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-cyano-2-methylenepentanoic acid

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Technology Process of 5-cyano-2-methylenepentanoic acid

There total 9 articles about 5-cyano-2-methylenepentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 14918-21-9
5-hexynonitrile

: 201230-82-2
carbon monoxide

: 108-98-5
thiophenol

: 147766-06-1
5-cyano-2-methylenepentanoic acid

: 5-Cyano-2-methylene-pentanethioic acid S-phenyl ester

Guidance literature:: With toluene-4-sulfonic acid; palladium diacetate; 1,3-bis-(diphenylphosphino)propane; In tetrahydrofuran; at 110 ℃; for 6h; under 15514.4 Torr;
DOI:10.1016/S0040-4039(00)02169-9

Reference yield: 84.0%

: 14918-21-9
5-hexynonitrile

: 201230-82-2
carbon monoxide

: 106-45-6
para-thiocresol

: 147766-06-1
5-cyano-2-methylenepentanoic acid

: 2-(3-cyano-propyl)-thioacrylic acid S-p-tolyl ester

Guidance literature:: With toluene-4-sulfonic acid; palladium diacetate; 1,3-bis-(diphenylphosphino)propane; In tetrahydrofuran; at 110 ℃; for 6h; under 15514.4 Torr;
DOI:10.1016/S0040-4039(00)02169-9

Reference yield: 76.0%

: 14918-21-9
5-hexynonitrile

: 124-38-9,18923-20-1
carbon dioxide

: 147766-06-1
5-cyano-2-methylenepentanoic acid

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; phenylsilane; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; In N,N-dimethyl-formamide; at 80 ℃; for 12h; under 15001.5 Torr; regioselective reaction;
DOI:10.1021/acscatal.0c01687