(2R)-3-cyclopentyl-2-({formyl[(phenylmethyl)oxy]amino}methyl)propanoic acid diisopropylethylamine salt

Base Information

Chemical Name:(2R)-3-cyclopentyl-2-({formyl[(phenylmethyl)oxy]amino}methyl)propanoic acid diisopropylethylamine salt
CAS No.:1152109-84-6
Molecular Formula:C₈H₁₉N*C₁₇H₂₃NO₄
Molecular Weight:434.619
Hs Code.:

Synonyms:(2R)-3-cyclopentyl-2-({formyl[(phenylmethyl)oxy]amino}methyl)propanoic acid diisopropylethylamine salt

Suppliers and Price of (2R)-3-cyclopentyl-2-({formyl[(phenylmethyl)oxy]amino}methyl)propanoic acid diisopropylethylamine salt

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2R)-3-cyclopentyl-2-({formyl[(phenylmethyl)oxy]amino}methyl)propanoic acid diisopropylethylamine salt

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2R)-3-cyclopentyl-2-({formyl[(phenylmethyl)oxy]amino}methyl)propanoic acid diisopropylethylamine salt

There total 10 articles about (2R)-3-cyclopentyl-2-({formyl[(phenylmethyl)oxy]amino}methyl)propanoic acid diisopropylethylamine salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7087-68-5
N-ethyl-N,N-diisopropylamine

: 301684-75-3
(2R)-3-cyclopentyl-2-({formyl[(phenylmethyl)oxy]amino}methyl)propanoic acid

: 1152109-84-6
(2R)-3-cyclopentyl-2-({formyl[(phenylmethyl)oxy]amino}methyl)propanoic acid diisopropylethylamine salt

Guidance literature:: In diethyl ether; at 20 ℃; for 3h;

Reference yield:

: 301685-09-6
(2R)-3-cyclopentyl-2-(hydroxymethyl)propanoic acid

: 1152109-84-6
(2R)-3-cyclopentyl-2-({formyl[(phenylmethyl)oxy]amino}methyl)propanoic acid diisopropylethylamine salt

Guidance literature:: Multi-step reaction with 5 steps

1.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 3 h / 0 °C / Inert atmosphere

2.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0.75 h / 0 °C / Inert atmosphere

3.1: lithium hydroxide monohydrate; water / tetrahydrofuran / 36 h / 20 °C / Inert atmosphere

4.1: acetic anhydride / dichloromethane / 0.75 h / 0 °C / Inert atmosphere

4.2: 1.5 h / 0 °C

5.1: diethyl ether / 3 h / 20 °C / Inert atmosphere

With dmap; lithium hydroxide monohydrate; di-isopropyl azodicarboxylate; water; acetic anhydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triphenylphosphine; In tetrahydrofuran; diethyl ether; dichloromethane;

Reference yield:

: 301685-10-9
(2R)-3-cyclopentyl-2-(hydroxymethyl)-N-[(phenylmethyl)oxy]propanamide

: 1152109-84-6
(2R)-3-cyclopentyl-2-({formyl[(phenylmethyl)oxy]amino}methyl)propanoic acid diisopropylethylamine salt

Guidance literature:: Multi-step reaction with 4 steps

1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0.75 h / 0 °C / Inert atmosphere

2.1: lithium hydroxide monohydrate; water / tetrahydrofuran / 36 h / 20 °C / Inert atmosphere

3.1: acetic anhydride / dichloromethane / 0.75 h / 0 °C / Inert atmosphere

3.2: 1.5 h / 0 °C

4.1: diethyl ether / 3 h / 20 °C / Inert atmosphere

With lithium hydroxide monohydrate; di-isopropyl azodicarboxylate; water; acetic anhydride; triphenylphosphine; In tetrahydrofuran; diethyl ether; dichloromethane;