Tris<butyl> isocyanurate

Base Information

Chemical Name:Tris<butyl> isocyanurate
CAS No.:153756-36-6
Molecular Formula:C₄₈H₆₀N₆O₁₅
Molecular Weight:961.036
Hs Code.:

Tris<<N-succinoyl-N-(benzyloxy)amino>butyl> isocyanurate

Synonyms:Tris<butyl> isocyanurate

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Chemical Property of Tris<butyl> isocyanurate

Chemical Property:

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Technology Process of Tris<butyl> isocyanurate

There total 4 articles about Tris<butyl> isocyanurate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 108-30-5
succinic acid anhydride

: 153756-35-5
Tris<-N-(benzyloxy)amino>butyl> isocyanurate

: 153756-36-6
Tris<butyl> isocyanurate

Guidance literature:: With acetic acid; zinc; In tetrahydrofuran; at 20 ℃; for 20h;
DOI:10.1016/S0968-0896(99)00248-5

Reference yield: 71.0%

: 108-30-5
succinic acid anhydride

: 153756-35-5
Tris<-N-(benzyloxy)amino>butyl> isocyanurate

: 153756-36-6
Tris<butyl> isocyanurate

: [bis[N-succinoyl]mono[N-(trichloroethoxy)carbonyl](benzyloxy)aminobutyl] isocyanurate

: 261783-74-8
[mono[N-succinoyl]bis[N-(trichloroethoxy)carbonyl](benzyloxy)aminobutyl] isocyanurate

Guidance literature:: With acetic acid; zinc; In tetrahydrofuran; at 35 - 40 ℃; for 8.5h;
DOI:10.1016/S0968-0896(99)00248-5

Reference yield:

: 90195-00-9
N-<(2,2,2-trichloroethoxy)carbonyl>-O-benzylhydroxylamine

: 153756-36-6
Tris<butyl> isocyanurate

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / NaH / dimethylformamide / Ambient temperature; 1.) 45 min, 2.) overnight

2: 85 percent / NaH, NaI / dimethylsulfoxide / Ambient temperature; 1.) 30 min, 2.) overnight

3: 90 percent / Zn, AcOH / tetrahydrofuran / Ambient temperature

With sodium hydride; acetic acid; sodium iodide; zinc; In tetrahydrofuran; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jo00084a018