Technology Process of C12H11NO4S
There total 3 articles about C12H11NO4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
3-(benzyloxy)isoxazole-5-carboxylic acid;
With
n-butyllithium;
In
tetrahydrofuran; hexane;
at -78 - 20 ℃;
for 1h;
Dimethyldisulphide;
In
tetrahydrofuran; hexane;
at -78 - 20 ℃;
for 2h;
With
hydrogenchloride; water;
In
tetrahydrofuran; hexane;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: methanol; lithium hydroxide; water / tetrahydrofuran / 14 h / 20 °C
2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 - 20 °C
2.2: 2 h / -78 - 20 °C
With
methanol; lithium hydroxide; n-butyllithium; water;
In
tetrahydrofuran; hexane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 70 °C
1.2: 3 h / 70 °C
2.1: methanol; lithium hydroxide; water / tetrahydrofuran / 14 h / 20 °C
3.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 - 20 °C
3.2: 2 h / -78 - 20 °C
With
methanol; lithium hydroxide; n-butyllithium; water; potassium carbonate;
In
tetrahydrofuran; hexane; N,N-dimethyl-formamide;