tris(trideuterio-methyl)-methyl tin

Base Information

Chemical Name:tris(trideuterio-methyl)-methyl tin
CAS No.:39103-76-9
Molecular Formula:C₄H₁₂Sn
Molecular Weight:187.778
Hs Code.:

Synonyms:tris(trideuterio-methyl)-methyl tin

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Chemical Property of tris(trideuterio-methyl)-methyl tin

Chemical Property:

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Technology Process of tris(trideuterio-methyl)-methyl tin

There total 2 articles about tris(trideuterio-methyl)-methyl tin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 80048-64-2
tri(methyl-d3)stannyl chloride

: 16393-89-8
(methyl)3GeSn(methyl)3

: CH₃(C⁽²⁾H₃)2SnCl

: (CH₃)2(C⁽²⁾H₃)SnCl

: 1066-45-1
trimethyltin(IV)chloride

: 594-27-4
tetramethylstannane

: 39103-76-9
tris(trideuterio-methyl)-methyl tin

Guidance literature:: In methanol; a mixt. of Me3GeSnMe3 and (CD3)3SnCl in methanol was kept for 15 h, reaction was followed by (1)H NMR spectroscopy; Me3SnCl:Me2(CD3)SnCl:Me(CD3)2SnCl=1:1:1.5, Me4Sn:Me3SnCD3:Me2Sn(CD3)2:MeSn(CD3)3=1:1.5:3.4:10; further products; not isolated, identified by (1)H NMR spectrum;
DOI:10.1016/0022-328X(85)80065-6

Reference yield:

: 80048-64-2
tri(methyl-d3)stannyl chloride

: 16393-89-8
(methyl)3GeSn(methyl)3

: chlorodimethyl(trimethylgermyl)stannane

: 1529-47-1
chlorotrimethylgermane

: 1449-63-4
trimethylgermane

: 58529-40-1
1,2-dichloro-tetramethyl-distannane

: 39103-76-9
tris(trideuterio-methyl)-methyl tin

Guidance literature:: In methanol; byproducts: Me(CD3)2SnCl; a mixt. of Me3GeSnMe3 and (CD3)3SnCl in methanol was kept for 220 min, reaction was followed by (1)H NMR spectroscopy; no Me2SnHCl, Me2SnCl2, and "dimethyltin polymer" were observed; first order behaviour up to 60% reaction, rate const. is given; not isolated, identified by (1)H and (2)H NMR spectra; Kinetics;
DOI:10.1016/0022-328X(85)80065-6