1-(trimethylsilyl)-2-methyl-2-trimethylsiloxy-1-aza-2-silacyclopentane

Base Information

• Chemical Name: 1-(trimethylsilyl)-2-methyl-2-trimethylsiloxy-1-aza-2-silacyclopentane
• CAS No.: 1616272-42-4
• Molecular Formula: C₁₀H₂₇NOSi₃
• Molecular Weight: 261.587

Synonyms:1-(trimethylsilyl)-2-methyl-2-trimethylsiloxy-1-aza-2-silacyclopentane

Chemical Property of 1-(trimethylsilyl)-2-methyl-2-trimethylsiloxy-1-aza-2-silacyclopentane

Chemical Property:

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Technology Process of 1-(trimethylsilyl)-2-methyl-2-trimethylsiloxy-1-aza-2-silacyclopentane

There total 2 articles about 1-(trimethylsilyl)-2-methyl-2-trimethylsiloxy-1-aza-2-silacyclopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.7%

1,1,1,3-tetramethyl-3-methoxy-3-(3-aminopropyl)disiloxane (1616272-43-5) + 1,1,1,3,3,3-hexamethyl-disilazane (999-97-3) → Trimethylmethoxysilane (1825-61-2) + 1-(trimethylsilyl)-2-methyl-2-trimethylsiloxy-1-aza-2-silacyclopentane (1616272-42-4)

Guidance literature:

With ammonium chloride; at 125 ℃; for 24h;

DOI:10.1134/S1070363214050168

Reference yield: 48.0%

Hexamethyldisiloxane (107-46-0) + 1-(trimethylsilyl)-2-methyl-2-methoxy-1-aza-2-silacyclopentane (1194232-88-6) → Trimethylmethoxysilane (1825-61-2) + 1-(trimethylsilyl)-2-methyl-2-trimethylsiloxy-1-aza-2-silacyclopentane (1616272-42-4)

Guidance literature:

With potassium hydroxide; at 120 ℃;

DOI:10.1134/S1070363214050168

Reference yield: 24.0%

1-(trimethylsilyl)-2-methyl-2-trimethylsiloxy-1-aza-2-silacyclopentane (1616272-42-4) + 1-(trimethylsilyl)-2-methyl-2-methoxy-1-aza-2-silacyclopentane (1194232-88-6) → Trimethylmethoxysilane (1825-61-2) + 2,2'-oxybis-[1-(trimethylsilyl)-2-methyl-1-aza-2-silacyclopentane] (1616272-44-6)

Guidance literature:

With sodium trimethylsilanolate; at 160 ℃; for 15h;

DOI:10.1134/S1070363214050168

upstream raw materials:

Hexamethyldisiloxane

1-(trimethylsilyl)-2-methyl-2-methoxy-1-aza-2-silacyclopentane

1,1,1,3-tetramethyl-3-methoxy-3-(3-aminopropyl)disiloxane

1,1,1,3,3,3-hexamethyl-disilazane

Downstream raw materials:

Trimethylmethoxysilane

2,2'-oxybis-[1-(trimethylsilyl)-2-methyl-1-aza-2-silacyclopentane]

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