N-(4-tert-butyldimethylsiloxy-2-methoxybenzyl)-3-allyl-4-methoxy-2,5-dimethoxymethoxyaniline

Base Information

Chemical Name:N-(4-tert-butyldimethylsiloxy-2-methoxybenzyl)-3-allyl-4-methoxy-2,5-dimethoxymethoxyaniline
CAS No.:1341219-92-8
Molecular Formula:C₂₈H₄₃NO₇Si
Molecular Weight:533.737
Hs Code.:

Synonyms:N-(4-tert-butyldimethylsiloxy-2-methoxybenzyl)-3-allyl-4-methoxy-2,5-dimethoxymethoxyaniline

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Chemical Property of N-(4-tert-butyldimethylsiloxy-2-methoxybenzyl)-3-allyl-4-methoxy-2,5-dimethoxymethoxyaniline

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Technology Process of N-(4-tert-butyldimethylsiloxy-2-methoxybenzyl)-3-allyl-4-methoxy-2,5-dimethoxymethoxyaniline

There total 4 articles about N-(4-tert-butyldimethylsiloxy-2-methoxybenzyl)-3-allyl-4-methoxy-2,5-dimethoxymethoxyaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₈H₄₁NO₇Si

: 1341219-92-8
N-(4-tert-butyldimethylsiloxy-2-methoxybenzyl)-3-allyl-4-methoxy-2,5-dimethoxymethoxyaniline

Guidance literature:: With sodium tris(acetoxy)borohydride; In dichloromethane; at 0 - 20 ℃; for 0.333333h;
DOI:10.1021/jo201495w

Reference yield:

: 129742-36-5
(4-((tert-butyldimethylsilyl)oxy)-2-methoxybenzaldehyde)

: 1341219-92-8
N-(4-tert-butyldimethylsiloxy-2-methoxybenzyl)-3-allyl-4-methoxy-2,5-dimethoxymethoxyaniline

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / dichloromethane / 0.17 h / 20 °C

2: sodium tris(acetoxy)borohydride / dichloromethane / 0.33 h / 0 - 20 °C

With sodium tris(acetoxy)borohydride; acetic acid; In dichloromethane;
DOI:10.1021/jo201495w

Reference yield:

: 18278-34-7
4-hydroxy-2-methoxybenzaldehyde

: 1341219-92-8
N-(4-tert-butyldimethylsiloxy-2-methoxybenzyl)-3-allyl-4-methoxy-2,5-dimethoxymethoxyaniline

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 0.5 h / 0 - 20 °C

2: acetic acid / dichloromethane / 0.17 h / 20 °C

3: sodium tris(acetoxy)borohydride / dichloromethane / 0.33 h / 0 - 20 °C

With 1H-imidazole; sodium tris(acetoxy)borohydride; acetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo201495w