methyl 3-acetoxy-4-(acetoxymethyl)-5-((4-methoxybenzyloxy)methyl)picolinate

Base Information

Chemical Name:methyl 3-acetoxy-4-(acetoxymethyl)-5-((4-methoxybenzyloxy)methyl)picolinate
CAS No.:1198621-61-2
Molecular Formula:C₂₁H₂₃NO₈
Molecular Weight:417.416
Hs Code.:

Synonyms:methyl 3-acetoxy-4-(acetoxymethyl)-5-((4-methoxybenzyloxy)methyl)picolinate

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Chemical Property of methyl 3-acetoxy-4-(acetoxymethyl)-5-((4-methoxybenzyloxy)methyl)picolinate

Chemical Property:

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Technology Process of methyl 3-acetoxy-4-(acetoxymethyl)-5-((4-methoxybenzyloxy)methyl)picolinate

There total 8 articles about methyl 3-acetoxy-4-(acetoxymethyl)-5-((4-methoxybenzyloxy)methyl)picolinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1198621-15-6
methyl 3-hydroxy-4-(hydroxymethyl)-5-((4-methoxybenzyloxy)methyl)picolinate

: 108-24-7
acetic anhydride

: 1198621-61-2
methyl 3-acetoxy-4-(acetoxymethyl)-5-((4-methoxybenzyloxy)methyl)picolinate

Guidance literature:: With triethylamine; dmap; In dichloromethane; for 3h;

Reference yield:

: 280762-58-5
5-{[(4-methoxybenzyl)oxy]methyl}-2,2-dimethyl-4H-[1,3]dioxino[4,5-c]pyridine-8-carbaldehyde

: 1198621-61-2
methyl 3-acetoxy-4-(acetoxymethyl)-5-((4-methoxybenzyloxy)methyl)picolinate

Guidance literature:: Multi-step reaction with 3 steps

1.1: iodine; potassium hydroxide / 0 - 23 °C

1.2: 4 h / 20 °C

2.1: formic acid / 1 h / 20 °C

3.1: triethylamine / dmap / dichloromethane / 3 h

With formic acid; iodine; triethylamine; potassium hydroxide; dmap; In dichloromethane;

Reference yield:

: 252987-04-5
(5-{[(4-methoxybenzyl)oxy]methyl}-2,2-dimethyl-4H-[1,3]dioxino[4,5-c]pyridin-8-yl)methanol

: 1198621-61-2
methyl 3-acetoxy-4-(acetoxymethyl)-5-((4-methoxybenzyloxy)methyl)picolinate

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 4 h / Reflux

2.1: iodine; potassium hydroxide / 0 - 23 °C

2.2: 4 h / 20 °C

3.1: formic acid / 1 h / 20 °C

4.1: triethylamine / dmap / dichloromethane / 3 h

With formic acid; iodine; triethylamine; potassium hydroxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; dmap; In dichloromethane; ethyl acetate;