(C₅(CH₃)5)Fe(PC₄H(CH₃)2CH₂C₅H₄)RuH(P(C₆H₅)3)

Base Information

Chemical Name:(C₅(CH₃)5)Fe(PC₄H(CH₃)2CH₂C₅H₄)RuH(P(C₆H₅)3)
CAS No.:341489-74-5
Molecular Formula:C₄₀H₄₄FeP₂Ru
Molecular Weight:743.654
Hs Code.:

(C<sub>5</sub>(CH<sub>3</sub>)5)Fe(PC<sub>4</sub>H(CH<sub>3</sub>)2CH<sub>2</sub>C<sub>5</sub>H<sub>4</sub>)RuH(P(C<sub>6</sub>H<sub>5</sub>)3)

Synonyms:(C₅(CH₃)5)Fe(PC₄H(CH₃)2CH₂C₅H₄)RuH(P(C₆H₅)3)

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Chemical Property of (C₅(CH₃)5)Fe(PC₄H(CH₃)2CH₂C₅H₄)RuH(P(C₆H₅)3)

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Technology Process of (C₅(CH₃)5)Fe(PC₄H(CH₃)2CH₂C₅H₄)RuH(P(C₆H₅)3)

There total 1 articles about (C₅(CH₃)5)Fe(PC₄H(CH₃)2CH₂C₅H₄)RuH(P(C₆H₅)3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 341489-70-1
(C₅(CH₃)5)Fe(PC₄H(CH₃)2CH₂C₅H₄)RuCl(P(C₆H₅)3)

: 341489-74-5
(C₅(CH₃)5)Fe(PC₄H(CH₃)2CH₂C₅H₄)RuH(P(C₆H₅)3)

Guidance literature:: With sodium methoxide; In methanol; toluene; under N2 atm. to soln. MeONa in MeOH was added soln. Cp*Fe(PC4HNe2CH2C5H4)RuCl(PPh3) in toluene and heated to reflux for 2 h; mixt. was evapd. to dryness, residue was chromed. on silica with 10:1 hexane/ether, solvent was removed;
DOI:10.1021/om0010262

Reference yield: 79.0%

: 60969-19-9
thallium(I) hexafluorophosphate

: 341489-74-5
(C₅(CH₃)5)Fe(PC₄H(CH₃)2CH₂C₅H₄)RuH(P(C₆H₅)3)

: 1333-74-0
hydrogen

: 55172-29-7,7791-12-0
thallium chloride

: 341489-77-8
(C₅(CH₃)5)Fe(PC₄H(CH₃)2CH₂C₅H₄)Ru(H₂)(P(C₆H₅)3)⁽¹⁺⁾*PF₆^(1-)=((C₅(CH₃)5)Fe(PC₄H(CH₃)2CH₂C₅H₄)Ru(H₂)(P(C₆H₅)3))PF₆

Guidance literature:: In dichloromethane; TlPF6 was added to soln. Cp*Fe(PC4HMe2CH2C5H4)RuCl(PPh3) in CH2Cl2 and stirred for 3 h under H2 atm. at room temp.; ppt. was filtered off, ether was to filtrate;
DOI:10.1021/om0010262