-6,6'-<1,4-phenylenebis(oxy)>bis-1,2-hexanediol

Base Information

Chemical Name:-6,6'-<1,4-phenylenebis(oxy)>bis-1,2-hexanediol
CAS No.:173427-91-3
Molecular Formula:C₁₈H₃₀O₆
Molecular Weight:342.433
Hs Code.:

<R-(R*,R*)>-6,6'-<1,4-phenylenebis(oxy)>bis-1,2-hexanediol

Synonyms:-6,6'-<1,4-phenylenebis(oxy)>bis-1,2-hexanediol

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Chemical Property of -6,6'-<1,4-phenylenebis(oxy)>bis-1,2-hexanediol

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Technology Process of -6,6'-<1,4-phenylenebis(oxy)>bis-1,2-hexanediol

There total 7 articles about -6,6'-<1,4-phenylenebis(oxy)>bis-1,2-hexanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

Na₂ SO₃: Na₂ SO₃

: 173427-90-2
1,4-di-(5-hexynyloxy)benzene

: 75-65-0
tert-butyl alcohol

: 173427-91-3
-6,6'-<1,4-phenylenebis(oxy)>bis-1,2-hexanediol

Guidance literature:: In water; ethyl acetate;

Reference yield: 62.0%

: 173427-90-2
1,4-di-(5-hexynyloxy)benzene

: 173427-91-3
-6,6'-<1,4-phenylenebis(oxy)>bis-1,2-hexanediol

Guidance literature:: With AD-mix-β;
DOI:10.1021/ja953781q

Reference yield:

: 173427-90-2
1,4-di-(5-hexynyloxy)benzene

: 173427-91-3
-6,6'-<1,4-phenylenebis(oxy)>bis-1,2-hexanediol

: (S)-6-[4-((S)-5,6-Dihydroxy-hexyloxy)-phenoxy]-hexane-1,2-diol

: (S)-6-[4-((R)-5,6-Dihydroxy-hexyloxy)-phenoxy]-hexane-1,2-diol

Guidance literature:: With potassium osmate(VI); hydroquinindine-2,5-diphenyl-4,6-pyrimidinediyl diether; potassium carbonate; potassium hexacyanoferrate(III); In water; tert-butyl alcohol; at 0 ℃; for 12h; Yield given; Yields of byproduct given. Title compound not separated from byproducts; other reagents: K₂Fe(CN)6 or I₂/(DHQD)2-PHAL or (DHQD)2-PYR or (DHQD)2-AQN/K₂CO₃/K₂OsO₄*2H₂O;
DOI:10.1021/jo980844p