N'-(8-(4-chlorophenyl)-1,6-naphthyridine-2-carbonyl)methanesulfonohydrazide

Base Information

Chemical Name:N'-(8-(4-chlorophenyl)-1,6-naphthyridine-2-carbonyl)methanesulfonohydrazide
CAS No.:1611472-29-7
Molecular Formula:C₁₆H₁₃ClN₄O₃S
Molecular Weight:376.823
Hs Code.:

Synonyms:N'-(8-(4-chlorophenyl)-1,6-naphthyridine-2-carbonyl)methanesulfonohydrazide

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Chemical Property of N'-(8-(4-chlorophenyl)-1,6-naphthyridine-2-carbonyl)methanesulfonohydrazide

Chemical Property:

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Technology Process of N'-(8-(4-chlorophenyl)-1,6-naphthyridine-2-carbonyl)methanesulfonohydrazide

There total 3 articles about N'-(8-(4-chlorophenyl)-1,6-naphthyridine-2-carbonyl)methanesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 1.0%

: 10393-86-9
methanesulphonyl hydrazide

: 1611473-57-4
8-(4-chlorophenyl)-1,6-naphthyridine-2-carboxylic acid

: 1611472-29-7
N'-(8-(4-chlorophenyl)-1,6-naphthyridine-2-carbonyl)methanesulfonohydrazide

Guidance literature:: 8-(4-chlorophenyl)-1,6-naphthyridine-2-carboxylic acid; With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

methanesulphonyl hydrazide; In N,N-dimethyl-formamide; for 5h;

Reference yield:

: 197507-55-4
8-bromo-[1,6]-naphthyridine-2-carboxylic acid

: 1611472-29-7
N'-(8-(4-chlorophenyl)-1,6-naphthyridine-2-carbonyl)methanesulfonohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1.1: caesium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane; water / 4 h / 80 °C

2.1: HATU; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 1 h / 20 °C

2.2: 5 h

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate; N-ethyl-N,N-diisopropylamine; HATU; In 1,4-dioxane; water; N,N-dimethyl-formamide;

Reference yield:

: 1679-18-1
4-Chlorophenylboronic acid

: 1611472-29-7
N'-(8-(4-chlorophenyl)-1,6-naphthyridine-2-carbonyl)methanesulfonohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1.1: caesium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane; water / 4 h / 80 °C

2.1: HATU; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 1 h / 20 °C

2.2: 5 h

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate; N-ethyl-N,N-diisopropylamine; HATU; In 1,4-dioxane; water; N,N-dimethyl-formamide;