triphenyl-phosphine oxide ; compound with 3,4,5,6-tetrachloro-pyrocatechol

Base Information

Chemical Name:triphenyl-phosphine oxide ; compound with 3,4,5,6-tetrachloro-pyrocatechol
CAS No.:22400-36-8
Molecular Formula:C₆H₂Cl₄O₂*C₁₈H₁₅OP
Molecular Weight:526.183
Hs Code.:

Synonyms:triphenyl-phosphine oxide ; compound with 3,4,5,6-tetrachloro-pyrocatechol

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Chemical Property of triphenyl-phosphine oxide ; compound with 3,4,5,6-tetrachloro-pyrocatechol

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Technology Process of triphenyl-phosphine oxide ; compound with 3,4,5,6-tetrachloro-pyrocatechol

There total 2 articles about triphenyl-phosphine oxide ; compound with 3,4,5,6-tetrachloro-pyrocatechol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 2435-53-2
o-tetrachloroquinone

: 65374-39-2
triphenylarsane selenide

: 22400-36-8
triphenyl-phosphine oxide ; compound with 3,4,5,6-tetrachloro-pyrocatechol

Guidance literature:: With water; In benzene; for 6h; Heating;

Reference yield: 80.0%

: 2435-53-2
o-tetrachloroquinone

: 3878-44-2
Triphenylphosphine selenide

: 22400-36-8
triphenyl-phosphine oxide ; compound with 3,4,5,6-tetrachloro-pyrocatechol

Guidance literature:: With water; In benzene; for 3h; Heating;

Reference yield: 95.0%

: 56-34-8
tetraethylammonium chloride

: 22400-36-8
triphenyl-phosphine oxide ; compound with 3,4,5,6-tetrachloro-pyrocatechol

: 1074-29-9
trichlorophenylgermane

: 99901-38-9
tetraethylammonium bis(3,4,5,6-tetrachloro-1,2-benzenediolato)phenylgermanate(IV)

Guidance literature:: With triethyl amine; In benzene; byproducts: triethylammonium chloride, triphenylphosphine oxide; addn. of adduct the and Et3N to soln. of GePhCl3, stirred at room temp. for 15 min; refluxed for 1h; filtered, evapd.; residue dissolved in CH3CN; addn. of Et4NCl; stirred for 10 min.; solvent evapd.; residue washed with water;; dried in vac., treated with benzene at room temp., stirred, filtered, washed with hexane, dissolved in boiling CH3CN, filtered, cooled down, pptn.; elem. anal.;;