tetraethylammonium bis(3,4,5,6-tetrachloro-1,2-benzenediolato)phenylgermanate(IV)

Base Information

Chemical Name:tetraethylammonium bis(3,4,5,6-tetrachloro-1,2-benzenediolato)phenylgermanate(IV)
CAS No.:99901-38-9
Molecular Formula:C₈H₂₀N*C₁₈H₅Cl₈GeO₄
Molecular Weight:771.703
Hs Code.:

Synonyms:tetraethylammonium bis(3,4,5,6-tetrachloro-1,2-benzenediolato)phenylgermanate(IV)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetraethylammonium bis(3,4,5,6-tetrachloro-1,2-benzenediolato)phenylgermanate(IV)

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Technology Process of tetraethylammonium bis(3,4,5,6-tetrachloro-1,2-benzenediolato)phenylgermanate(IV)

There total 1 articles about tetraethylammonium bis(3,4,5,6-tetrachloro-1,2-benzenediolato)phenylgermanate(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 56-34-8
tetraethylammonium chloride

: 22400-36-8
triphenyl-phosphine oxide ; compound with 3,4,5,6-tetrachloro-pyrocatechol

: 1074-29-9
trichlorophenylgermane

: 99901-38-9
tetraethylammonium bis(3,4,5,6-tetrachloro-1,2-benzenediolato)phenylgermanate(IV)

Guidance literature:: With triethyl amine; In benzene; byproducts: triethylammonium chloride, triphenylphosphine oxide; addn. of adduct the and Et3N to soln. of GePhCl3, stirred at room temp. for 15 min; refluxed for 1h; filtered, evapd.; residue dissolved in CH3CN; addn. of Et4NCl; stirred for 10 min.; solvent evapd.; residue washed with water;; dried in vac., treated with benzene at room temp., stirred, filtered, washed with hexane, dissolved in boiling CH3CN, filtered, cooled down, pptn.; elem. anal.;;