4-<2-<(carbobenzyloxy)methylamino>ethyl>-4-<2-(allyloxy)-3-methoxyphenyl>-2-cyclohexenone

Base Information

Chemical Name:4-<2-<(carbobenzyloxy)methylamino>ethyl>-4-<2-(allyloxy)-3-methoxyphenyl>-2-cyclohexenone
CAS No.:80754-82-1
Molecular Formula:C₂₇H₃₁NO₅
Molecular Weight:449.547
Hs Code.:

Synonyms:4-<2-<(carbobenzyloxy)methylamino>ethyl>-4-<2-(allyloxy)-3-methoxyphenyl>-2-cyclohexenone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-<2-<(carbobenzyloxy)methylamino>ethyl>-4-<2-(allyloxy)-3-methoxyphenyl>-2-cyclohexenone

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Technology Process of 4-<2-<(carbobenzyloxy)methylamino>ethyl>-4-<2-(allyloxy)-3-methoxyphenyl>-2-cyclohexenone

There total 14 articles about 4-<2-<(carbobenzyloxy)methylamino>ethyl>-4-<2-(allyloxy)-3-methoxyphenyl>-2-cyclohexenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23343-06-8
2-allyloxy-3-methoxy-benzaldehyde

: 80754-82-1
4-<2-<(carbobenzyloxy)methylamino>ethyl>-4-<2-(allyloxy)-3-methoxyphenyl>-2-cyclohexenone

Guidance literature:: Multi-step reaction with 5 steps

2: pyridinium dichromate / dimethylformamide / 1.) 0 deg C, 0.5 h, 2.) RT, 4 h

4: 1N HCl / 6 h / Ambient temperature

5: 10percent KOH / methanol / 2 h / Ambient temperature

With hydrogenchloride; potassium hydroxide; dipyridinium dichromate; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jo00347a029

Reference yield:

: 78166-98-0
1-<2-(allyloxy)-3-methoxyphenyl>-2-propenone

: 80754-82-1
4-<2-<(carbobenzyloxy)methylamino>ethyl>-4-<2-(allyloxy)-3-methoxyphenyl>-2-cyclohexenone

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / camphorsulfonic acid / 36 h / Ambient temperature

2: n-butyllithium / tetrahydrofuran / 2 h / Heating

3: 2.) HMPA / 1.) THF, -78 deg C, 1 h, 2.) THF, RT

4: 1N HCl / 6 h / Ambient temperature

5: 10percent KOH / methanol / 2 h / Ambient temperature

With hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hydroxide; n-butyllithium; camphor-10-sulfonic acid; In tetrahydrofuran; methanol;
DOI:10.1021/jo00347a029

Reference yield:

: 30379-59-0
benzyl N-methylcarbamate

: 80754-82-1
4-<2-<(carbobenzyloxy)methylamino>ethyl>-4-<2-(allyloxy)-3-methoxyphenyl>-2-cyclohexenone

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / Camphorsulfonic Acid / 25 °C

2: n-Butyllithium

3: 0.5N KOH / methanol; H₂O / 2 h / 25 °C

With potassium hydroxide; n-butyllithium; camphor-10-sulfonic acid; In methanol; water;
DOI:10.1021/jo00330a045