[7-(4-fluorophenyl)-8-hydrazino-7H-12-oxa-9,11-diazabenzo[a]anthracen-10-yl]dimethylamine

Base Information

• Chemical Name: [7-(4-fluorophenyl)-8-hydrazino-7H-12-oxa-9,11-diazabenzo[a]anthracen-10-yl]dimethylamine
• CAS No.: 916079-59-9
• Molecular Formula: C₂₃H₂₀FN₅O
• Molecular Weight: 401.443

Synonyms:[7-(4-fluorophenyl)-8-hydrazino-7H-12-oxa-9,11-diazabenzo[a]anthracen-10-yl]dimethylamine

Chemical Property of [7-(4-fluorophenyl)-8-hydrazino-7H-12-oxa-9,11-diazabenzo[a]anthracen-10-yl]dimethylamine

Chemical Property:

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Technology Process of [7-(4-fluorophenyl)-8-hydrazino-7H-12-oxa-9,11-diazabenzo[a]anthracen-10-yl]dimethylamine

There total 4 articles about [7-(4-fluorophenyl)-8-hydrazino-7H-12-oxa-9,11-diazabenzo[a]anthracen-10-yl]dimethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

[8-chloro-7-(4-fluorophenyl)-7H-12-oxa-9,11-diazabenzo[a]anthracen-10-yl]dimethylamine (916079-55-5) → [7-(4-fluorophenyl)-8-hydrazino-7H-12-oxa-9,11-diazabenzo[a]anthracen-10-yl]dimethylamine (916079-59-9)

Guidance literature:

With hydrazine hydrate; In ethanol; N,N-dimethyl-formamide; for 8h; Heating;

DOI:10.1515/HC.2006.12.1.73

Reference yield:

α-naphthol (90-15-3) → [7-(4-fluorophenyl)-8-hydrazino-7H-12-oxa-9,11-diazabenzo[a]anthracen-10-yl]dimethylamine (916079-59-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 78 percent / piperidine / ethanol / 5 h / Heating

2: 91 percent / 1,2-dichloro-ethane / 20 °C

3: 88 percent / hydrazine hydrate / ethanol; dimethylformamide / 8 h / Heating

With piperidine; hydrazine hydrate; In ethanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

DOI:10.1515/HC.2006.12.1.73

Reference yield:

4-fluorobenzylidenemalononitrile (2826-22-4) → [7-(4-fluorophenyl)-8-hydrazino-7H-12-oxa-9,11-diazabenzo[a]anthracen-10-yl]dimethylamine (916079-59-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 78 percent / piperidine / ethanol / 5 h / Heating

2: 91 percent / 1,2-dichloro-ethane / 20 °C

3: 88 percent / hydrazine hydrate / ethanol; dimethylformamide / 8 h / Heating

With piperidine; hydrazine hydrate; In ethanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

DOI:10.1515/HC.2006.12.1.73

upstream raw materials:

[8-chloro-7-(4-fluorophenyl)-7H-12-oxa-9,11-diazabenzo[a]anthracen-10-yl]dimethylamine

α-naphthol

4-fluorobenzylidenemalononitrile

2-amino-4-(4-fluorophenyl)-4H-benzo[h]chromene-3-carbonitrile

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