C₁₆H₁₃BrO₄

Base Information

Chemical Name:C₁₆H₁₃BrO₄
CAS No.:1254348-94-1
Molecular Formula:C₁₆H₁₃BrO₄
Molecular Weight:349.181
Hs Code.:

C<sub>16</sub>H<sub>13</sub>BrO<sub>4</sub>

Synonyms:C₁₆H₁₃BrO₄

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Chemical Property of C₁₆H₁₃BrO₄

Chemical Property:

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Technology Process of C₁₆H₁₃BrO₄

There total 11 articles about C₁₆H₁₃BrO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1254346-10-5
phenyl 4-formyl-2-methoxy-6-methylbenzoate

: 1254348-94-1
C₁₆H₁₃BrO₄

Guidance literature:: With bromine; acetic acid; at 20 ℃; for 1h;

Reference yield:

: 877149-05-8
4-bromo-2-methoxy-6-methyl-benzonitrile

: 1254348-94-1
C₁₆H₁₃BrO₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: diisobutylaluminium hydride / toluene; tetrahydrofuran / -78 - 20 °C

1.2: 0 - 20 °C

2.1: 2-methyl-but-2-ene; water; sodium chlorite; sodium dihydrogenphosphate / tert-butyl alcohol / 0.5 h / 20 °C

2.2: pH 1

3.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

4.1: dmap; triethylamine / dichloromethane / 1 h / 20 °C

5.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 19 h / Inert atmosphere; Reflux

6.1: ozone; oxygen / dichloromethane / -78 °C

6.2: -78 - 25 °C

7.1: bromine; acetic acid / 1 h / 20 °C

With dmap; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; oxalyl dichloride; water; bromine; oxygen; diisobutylaluminium hydride; potassium carbonate; ozone; acetic acid; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; toluene; tert-butyl alcohol;

Reference yield:

: 877149-08-1
4-bromo-2-methoxy-6-methyl-benzoic acid

: 1254348-94-1
C₁₆H₁₃BrO₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

2.1: dmap; triethylamine / dichloromethane / 1 h / 20 °C

3.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 19 h / Inert atmosphere; Reflux

4.1: ozone; oxygen / dichloromethane / -78 °C

4.2: -78 - 25 °C

5.1: bromine; acetic acid / 1 h / 20 °C

With dmap; oxalyl dichloride; bromine; oxygen; potassium carbonate; ozone; acetic acid; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N,N-dimethyl-formamide; In 1,4-dioxane; dichloromethane; water;